1,3-Benzodioxole, 2-chloro-

Base Information

• Chemical Name: 1,3-Benzodioxole, 2-chloro-
• CAS No.: 24956-33-0
• Molecular Formula: C7H5ClO2
• Molecular Weight: 156.569
• Hs Code.: 2932999099
• Mol file: 24956-33-0.mol

Synonyms:2-Chlor-1,3-benzodioxol;

Chemical Property of 1,3-Benzodioxole, 2-chloro-

Chemical Property:

• Boiling Point: 62-63 °C(Press: 0.5 Torr)
• PSA: 18.46000
• Density: 1.39±0.1 g/cm3(Predicted)
• LogP: 1.98020

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,3-Benzodioxole, 2-chloro-

There total 1 articles about 1,3-Benzodioxole, 2-chloro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 2-chloro-benzo[1,3]dioxole (24956-33-0)

Guidance literature:

2-Acetoxy-1,3-benzodioxol;

DOI:10.1016/S0040-4039(01)88869-9

Reference yield: 58.0%

2-chloro-benzo[1,3]dioxole (24956-33-0) + sodium-manganese pentacarbonyl (13859-41-1) → (C6H4O2)CHMn(CO)5 + sodium chloride (7647-14-5)

Guidance literature:

In tetrahydrofuran; under N2; soln. of 5mmol NaMn(CO)5 in THF cooled to -78°C, 5.25 mmol C6H4O2CHCl added; mixt. warmed up to room temp., then stirred for 12 h; pptd. NaCl filtered off, solvent removed; residue extd. with pentane; pentane soln. cooled, ppt. recrystd. from pentane; elem anal.;

Downstream raw materials:

sodium chloride