7-Nonen-2-one, (E)-

Base Information

• Chemical Name: 7-Nonen-2-one, (E)-
• CAS No.: 25143-93-5
• Molecular Formula: C9H16O
• Molecular Weight: 140.225
• Mol file: 25143-93-5.mol

Synonyms:

Chemical Property of 7-Nonen-2-one, (E)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 7-Nonen-2-one, (E)-

There total 1 articles about 7-Nonen-2-one, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-Acetyl-2-methylcyclohexanone (37457-18-4) → 1-(2-methylcyclohexyl)ethanone (64811-81-0) + (Z)-non-7-en-2-one (63196-65-6) + non-7t-en-2-one (25143-93-5)

Guidance literature:

With hydrogenchloride; mercury; zinc; for 0.75h; Title compound not separated from byproducts; Heating;

DOI:10.1071/CH9951827

Reference yield:

non-7t-en-2-one (25143-93-5) → (R)-1-((1S,2R)-2-Amino-2-methyl-cyclohexyl)-ethanol

Guidance literature:

Multi-step reaction with 3 steps

1.1: benzene / 20 h / Heating

2.1: TEA / CH₂Cl₂ / 0 - 20 °C

2.2: 3 Angstroem molecular sieves; TFA / 1,2-dichloro-ethane / 0 - 20 °C

2.3: BF₃ etherate / 1,2-dichloro-ethane; methoxybenzene / 18 h / Heating

3.1: H₂ / Pd(OH)2/C / ethyl acetate / 15 h / 100 °C / 54300.5 Torr

With TEA; hydrogen; palladium dihydroxide; In dichloromethane; ethyl acetate; benzene; 2.2: intramolecular Diels-Alder reaction / 2.3: intramolecular Diels-Alder reaction;

DOI:10.1021/ol035046m

Reference yield:

non-7t-en-2-one (25143-93-5) → 4,8a-dimethyl-2-phenyl-4a,5,6,7,8,8a-hexahydro-4H-benzo[d][1,3]oxazine

Guidance literature:

Multi-step reaction with 2 steps

1.1: benzene / 20 h / Heating

2.1: TEA / CH₂Cl₂ / 0 - 20 °C

2.2: 3 Angstroem molecular sieves; TFA / 1,2-dichloro-ethane / 0 - 20 °C

2.3: BF₃ etherate / 1,2-dichloro-ethane; methoxybenzene / 18 h / Heating

With TEA; In dichloromethane; benzene; 2.2: intramolecular Diels-Alder reaction / 2.3: intramolecular Diels-Alder reaction;

DOI:10.1021/ol035046m

upstream raw materials:

3-Acetyl-2-methylcyclohexanone