Benzoyl chloride 4-chlorophenylhydrazone

Base Information

• Chemical Name: Benzoyl chloride 4-chlorophenylhydrazone
• CAS No.: 17359-82-9
• Molecular Formula: C13H10 Cl2 N2
• Molecular Weight: 265.142
• Hs Code.: 2928000090
• ChEMBL ID: CHEMBL150320
• Mol file: 17359-82-9.mol

Synonyms:Benzoyl chloride 4-chlorophenylhydrazone;17359-82-9;N-(4-Chlorophenyl)benzenecarbohydrazonoylchloride;BRN 0649820;BENZOYL CHLORIDE, (p-CHLOROPHENYL)HYDRAZONE;(Z)-N-(4-CHLOROPHENYL)BENZENECARBOHYDRAZONOYL CHLORIDE;N-(4-Chlorophenyl)benzenecarbohydrazonoyl chloride;C13H10Cl2N2;CHEMBL150320;AKOS000281763;LS-42596;A811536;amino-(4-chlorophenyl)-[chloro(phenyl)methylene]ammonium

Chemical Property of Benzoyl chloride 4-chlorophenylhydrazone

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Melting Point: 106 °C
• Boiling Point: 371.2°Cat760mmHg
• PKA: 14.39±0.10(Predicted)
• Flash Point: 178.3°C
• PSA: 24.39000
• Density: 1.24g/cm³
• LogP: 4.42550
• XLogP3: 5.2
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 3
• Exact Mass: 264.0221037
• Heavy Atom Count: 17
• Complexity: 254

Purity/Quality:

97% ^*data from raw suppliers

N-(4-Chlorophenyl)benzenecarbohydrazonoylchloride 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C(=NNC2=CC=C(C=C2)Cl)Cl
• Isomeric SMILES: C1=CC=C(C=C1)/C(=N/NC2=CC=C(C=C2)Cl)/Cl

Technology Process of Benzoyl chloride 4-chlorophenylhydrazone

There total 14 articles about Benzoyl chloride 4-chlorophenylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

<(p-chlorophenyl)azo>stilbene (88267-39-4) → benzaldehyde (100-52-7) + N-(α-chlorobenzylidene)-N'-p-chlorophenylhydrazine (17359-82-9)

Guidance literature:

With CuCl₂*2H₂O; In acetone; at 0 ℃; for 1h;

Reference yield:

benzaldehyde-p-chlorophenylhydrazone (2833-68-3) → N-(α-chlorobenzylidene)-N'-p-chlorophenylhydrazine (17359-82-9)

Guidance literature:

With N-chloro-succinimide; dimethylsulfide; In dichloromethane; at -78 ℃; for 1h;

DOI:10.1016/j.ejmech.2017.09.037

Reference yield:

N'-(4-chlorophenyl)benzohydrazide (17473-76-6) → (Z)-N'-(4-chlorophenyl)benzohydrazonoyl chloride (17359-82-9)

Guidance literature:

With tetrachloromethane; triphenylphosphine; In acetonitrile; at 20 ℃;

DOI:10.1021/ol502515b

upstream raw materials:

<(p-chlorophenyl)azo>stilbene

benzaldehyde phenylhydrazone

N'-(4-chlorophenyl)benzohydrazide

N-4-chlorophenylhydrazine

Downstream raw materials:

1-(4-chloro-phenyl)-3-phenyl-(3ar,8bc)-3a,8b-dihydro-1H-benzo[4,5]thieno[3,2-c]pyrazole 4,4-dioxide

C₁₅H₁₆ClN₃

C₁₉H₂₄ClN₃

[3-(4-chloro-phenyl)-5-phenyl-3H-[1,3,4]thiadiazol-2-ylidene]-dimethyl-urea