2H-Pyran, 3,4-dihydro-6-(4-methoxyphenyl)-

Base Information

Chemical Name:2H-Pyran, 3,4-dihydro-6-(4-methoxyphenyl)-
CAS No.:25882-22-8
Molecular Formula:C12H14O2
Molecular Weight:190.242
Hs Code.:
DSSTox Substance ID:DTXSID10437469
Nikkaji Number:J651.368I
Mol file:25882-22-8.mol

Synonyms:2H-Pyran, 3,4-dihydro-6-(4-methoxyphenyl)-;25882-22-8;2-(4-methoxyphenyl)-5,6-dihydro-4H-pyran;DTXSID10437469

Suppliers and Price of 2H-Pyran, 3,4-dihydro-6-(4-methoxyphenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of 2H-Pyran, 3,4-dihydro-6-(4-methoxyphenyl)-

Chemical Property:

XLogP3:2.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:190.099379685
Heavy Atom Count:14
Complexity:202

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=C(C=C1)C2=CCCCO2

Technology Process of 2H-Pyran, 3,4-dihydro-6-(4-methoxyphenyl)-

There total 14 articles about 2H-Pyran, 3,4-dihydro-6-(4-methoxyphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 171364-79-7
2-(4-methoxyphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 626232-55-1
phosphoric acid 5,6-dihydro-4H-pyran-2-yl ester diphenyl ester

: 25882-22-8
4-<2-(5,6-Dihydro-4H-pyranyl)>anisole

Guidance literature:: phosphoric acid 5,6-dihydro-4H-pyran-2-yl ester diphenyl ester; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In tetrahydrofuran; at 22 ℃; Inert atmosphere;

2-(4-methoxyphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane; With sodium carbonate; In tetrahydrofuran; water; at 65 ℃; for 18h;
DOI:10.1016/j.tetlet.2013.10.031

Reference yield: 86.0%

: 5720-07-0
4-methoxyphenylboronic acid

: 626232-55-1
phosphoric acid 5,6-dihydro-4H-pyran-2-yl ester diphenyl ester

: 25882-22-8
4-<2-(5,6-Dihydro-4H-pyranyl)>anisole

Guidance literature:: With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In N,N-dimethyl-formamide; at 50 ℃; for 2.5h;
DOI:10.1016/j.tetlet.2008.04.116

Reference yield: 76.0%

: 104-92-7
1-bromo-4-methoxy-benzene

: 72081-15-3
6-lithio-3,4-dihydro-2H-pyran

: 25882-22-8
4-<2-(5,6-Dihydro-4H-pyranyl)>anisole

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; XPhos; In toluene; at 60 ℃; for 1h; Schlenk technique; Inert atmosphere;
DOI:10.1039/c4sc03117b