2-Cyano-N,N-diethylbenzamide

Base Information

Chemical Name:2-Cyano-N,N-diethylbenzamide
CAS No.:26487-09-2
Molecular Formula:C12H14N2O
Molecular Weight:202.256
Hs Code.:
DSSTox Substance ID:DTXSID40526214
Nikkaji Number:J3.456.267I
Wikidata:Q82394474

Synonyms:2-Cyano-N,N-diethylbenzamide;26487-09-2;DTXSID40526214

Suppliers and Price of 2-Cyano-N,N-diethylbenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 2-Cyano-N,N-diethylbenzamide

Chemical Property:

XLogP3:1.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:202.110613074
Heavy Atom Count:15
Complexity:262

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN(CC)C(=O)C1=CC=CC=C1C#N

Technology Process of 2-Cyano-N,N-diethylbenzamide

There total 4 articles about 2-Cyano-N,N-diethylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1696-17-9
N,N-diethylbenzamide

: 55305-43-6
N-cyano-N-phenyl-p-toluenesulfonamide

: 26487-09-2
2-cyano-N,N-diethylbenzamide

Guidance literature:: With silver hexafluoroantimonate; (p-cymene)ruthenium(II) chloride; sodium acetate; In 1,2-dichloro-ethane; at 120 ℃; for 24h; chemoselective reaction; Sealed tube; Inert atmosphere;
DOI:10.1039/c3cc49502g

Reference yield: 72.0%

: 7321-55-3
2,2-dimethylmalononitrile

: 1696-17-9
N,N-diethylbenzamide

: 26487-09-2
2-cyano-N,N-diethylbenzamide

Guidance literature:: N,N-diethylbenzamide; With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; In tetrahydrofuran; cyclohexane; at -78 ℃; for 1h;

2,2-dimethylmalononitrile; In tetrahydrofuran; at -78 - 23 ℃; for 3h;
DOI:10.1021/jacs.5b06136