(E)-N-(4-Methoxyphenyl)-1-(6-methylpyridin-2-yl)methanimine

Base Information

Chemical Name:(E)-N-(4-Methoxyphenyl)-1-(6-methylpyridin-2-yl)methanimine
CAS No.:26825-36-5
Molecular Formula:C14H14N2O
Molecular Weight:226.278
Hs Code.:
DSSTox Substance ID:DTXSID50514228
Nikkaji Number:J1.524.764I

Synonyms:26825-36-5;DTXSID50514228;(E)-N-(4-Methoxyphenyl)-1-(6-methylpyridin-2-yl)methanimine

Suppliers and Price of (E)-N-(4-Methoxyphenyl)-1-(6-methylpyridin-2-yl)methanimine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-N-(4-Methoxyphenyl)-1-(6-methylpyridin-2-yl)methanimine

Chemical Property:

XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:226.110613074
Heavy Atom Count:17
Complexity:247

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=NC(=CC=C1)C=NC2=CC=C(C=C2)OC

Technology Process of (E)-N-(4-Methoxyphenyl)-1-(6-methylpyridin-2-yl)methanimine

There total 2 articles about (E)-N-(4-Methoxyphenyl)-1-(6-methylpyridin-2-yl)methanimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1122-72-1
6-methyl-2-pyridinecarboxaldehyde

: 104-94-9
4-methoxy-aniline

: 26825-36-5
2-(C(H)=N-p-anisyl)-6-(Me)C₅H₃N

Guidance literature:: for 6h; Molecular sieve; Reflux;
DOI:10.1021/jacs.9b09395

Reference yield:

: 26825-36-5
2-(C(H)=N-p-anisyl)-6-(Me)C₅H₃N

Guidance literature:: 6-Methyl-2-hydroxymethylpyridin, p-Anisidin, Oxidmitteln;

Reference yield: 78.0%

: 26825-36-5
2-(C(H)=N-p-anisyl)-6-(Me)C₅H₃N

: 12257-42-0
[(norbornadiene)rhodium(I)chloride]2

: [RhCl(2-(C(H)=N-p-anisyl)-6-(Me)C₅H₃N)(bicyclo[2.2.1]hepta-2,5-diene)]

Guidance literature:: In dichloromethane; N2-atmosphere; addn. of imine (2 equiv.) to soln. of Rh-compd. (at 195 K), warming to room temp.; evapn. (vac.), washing (benzene, pentane), drying (vac.); elem. anal.;
DOI:10.1021/om960760b