4-Fluoro-cinnamyl chloride

Base Information

Chemical Name:4-Fluoro-cinnamyl chloride
CAS No.:27064-92-2
Molecular Formula:C9H8ClF
Molecular Weight:170.614
Hs Code.:
DSSTox Substance ID:DTXSID501265537

Synonyms:4-fluoro-cinnamyl chloride;3-(4-Fluorophenyl)allyl chloride;AVLSENGQODSCBK-UHFFFAOYSA-N;DTXSID501265537;AKOS017529185;3-(4-fluorophenyl)-2-propenyl chloride;1-(3-Chloro-1-propen-1-yl)-4-fluorobenzene

Suppliers and Price of 4-Fluoro-cinnamyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Fluoro-cinnamyl chloride

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:170.0298561
Heavy Atom Count:11
Complexity:126

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC(=CC=C1C=CCCl)F

Technology Process of 4-Fluoro-cinnamyl chloride

There total 9 articles about 4-Fluoro-cinnamyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 124980-95-6,7361-55-9
3-(4-fluorophenyl)prop-2-en-1-ol

: 27064-92-2
1-(3-chloro-1-propen-1-yl)-4-fluorobenzene

Guidance literature:: With thionyl chloride;
DOI:10.1039/j29660000590

Reference yield:

: 70090-77-6
1-fluoro-4-(propa-1,2-dien-1-yl)benzene

: 27064-92-2
1-(3-chloro-1-propen-1-yl)-4-fluorobenzene

: 1600528-33-3
(E)-1,2-dichloro-3-(4-fluorophenyl)-2-propene

: 1600528-36-6
2,3-dichloro-3-(4-fluorophenyl)-1-propene

: 1600528-30-0
(Z)-1,2-dichloro-3-(4-fluorophenyl)-2-propene

Guidance literature:: With chloro-trimethyl-silane; Selectfluor; 1-butyl-3-methylimidazolium Tetrafluoroborate; at 25 ℃; for 48h;
DOI:10.1016/j.tetlet.2014.02.110

Reference yield:

: 459-57-4
4-fluorobenzaldehyde

: 3536-96-7
vinylmagnesium chloride

: 27064-92-2
1-(3-chloro-1-propen-1-yl)-4-fluorobenzene

: 10335-90-7
1-(fluorophenyl)allyl chloride

Guidance literature:: 4-fluorobenzaldehyde; vinylmagnesium chloride; In tetrahydrofuran; at 0 ℃; for 0.0833333h; Inert atmosphere; Schlenk technique;

With hydrogenchloride; In diethyl ether; dichloromethane; at 20 ℃; Overall yield = 74 percent; Overall yield = 2.34 g; Inert atmosphere; Schlenk technique;
DOI:10.1021/jacs.9b04699