2-amino-N-(4-methylphenyl)benzenesulfonamide

Base Information

Chemical Name:2-amino-N-(4-methylphenyl)benzenesulfonamide
CAS No.:27384-96-9
Molecular Formula:C13H14N2O2S
Molecular Weight:262.332
Hs Code.:
DSSTox Substance ID:DTXSID80406420
Wikidata:Q82211373

Synonyms:2-amino-N-(4-methylphenyl)benzenesulfonamide;27384-96-9;Oprea1_146711;DTXSID80406420;AKOS000147003;2-AMINO-N-(4-METHYLPHENYL)-1-BENZENESULFONAMIDE

Suppliers and Price of 2-amino-N-(4-methylphenyl)benzenesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 2-amino-N-(4-methylphenyl)benzenesulfonamide

Chemical Property:

XLogP3:2.7
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:262.07759887
Heavy Atom Count:18
Complexity:356

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)NS(=O)(=O)C2=CC=CC=C2N

Technology Process of 2-amino-N-(4-methylphenyl)benzenesulfonamide

There total 4 articles about 2-amino-N-(4-methylphenyl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 63228-66-0
N-(4'-methylphenyl)-2-nitrobenzenesulfonamide

: 27384-96-9
2-amino-N-(4'-methylphenyl)benzenesulfonamide

Guidance literature:: With tin(II) chloride dihdyrate; In ethyl acetate; for 18h; Reflux;
DOI:10.1039/d1ob00968k

Reference yield:

: 1694-92-4
2-Nitrobenzenesulfonyl chloride

: 27384-96-9
2-amino-N-(4'-methylphenyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 6 h / 0 - 20 °C

2: tin(II) chloride dihdyrate / ethyl acetate / 18 h / Reflux

With tin(II) chloride dihdyrate; triethylamine; In dichloromethane; ethyl acetate;
DOI:10.1039/d1ob00968k

Reference yield:

: 106-49-0,12221-03-3
p-toluidine

: 27384-96-9
2-amino-N-(4'-methylphenyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 6 h / 0 - 20 °C

2: tin(II) chloride dihdyrate / ethyl acetate / 18 h / Reflux

With tin(II) chloride dihdyrate; triethylamine; In dichloromethane; ethyl acetate;
DOI:10.1039/d1ob00968k