2-Methoxy-5-nitrobenzophenone

Base Information

Chemical Name:2-Methoxy-5-nitrobenzophenone
CAS No.:2750-15-4
Molecular Formula:C₁₄H₁₁NO₄
Molecular Weight:257.246
Hs Code.:
DSSTox Substance ID:DTXSID90493205
Wikidata:Q82339732

Synonyms:2-methoxy-5-nitrobenzophenone;2750-15-4;DTXSID90493205;(2-Methoxy-5-nitrophenyl)(phenyl)methanone

Suppliers and Price of 2-Methoxy-5-nitrobenzophenone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 2-Methoxy-5-nitrobenzophenone

Chemical Property:

XLogP3:2.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:257.06880783
Heavy Atom Count:19
Complexity:333

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C(C=C1)[N+](=O)[O-])C(=O)C2=CC=CC=C2

Technology Process of 2-Methoxy-5-nitrobenzophenone

There total 6 articles about 2-Methoxy-5-nitrobenzophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 100-17-4
para-methoxynitrobenzene

: 36967-85-8
benzoyl triflate

: 2750-15-4
(2-methoxy-5-nitrophenyl)(phenyl)methanone

Guidance literature:: at 60 ℃; for 16h; Glovebox;
DOI:10.1002/anie.201814660

Reference yield:

: 532-32-1
sodium benzoate

: 2750-15-4
(2-methoxy-5-nitrophenyl)(phenyl)methanone

Guidance literature:: Multi-step reaction with 2 steps

1: iodine; carbon monoxide; bis(η3-allyl-μ-chloropalladium(II)); triphenylphosphine / 1,2-dichloro-ethane / 24 h / 20 °C / 3040.2 Torr / Sealed tube

2: 16 h / 60 °C / Glovebox

With bis(η3-allyl-μ-chloropalladium(II)); carbon monoxide; iodine; triphenylphosphine; In 1,2-dichloro-ethane; 2: |Friedel-Crafts Acylation;
DOI:10.1002/anie.201814660

Reference yield:

: 65-85-0,8013-63-6
benzoic acid

: 2750-15-4
(2-methoxy-5-nitrophenyl)(phenyl)methanone

Guidance literature:: Multi-step reaction with 2 steps

1: iodine; carbon monoxide / 1,2-dichloro-ethane / 24 h / 20 °C / 3040.2 Torr / Sealed tube

2: 16 h / 60 °C / Glovebox

With carbon monoxide; iodine; In 1,2-dichloro-ethane; 2: |Friedel-Crafts Acylation;
DOI:10.1002/anie.201814660