2,3-Dihydro-1H-inden-1-one semicarbazone

Base Information

• Chemical Name: 2,3-Dihydro-1H-inden-1-one semicarbazone
• CAS No.: 7461-24-7
• Molecular Formula: C₁₀H₁₁N₃O
• Molecular Weight: 189.217
• NSC Number: 404796
• Nikkaji Number: J656.993E
• Mol file: 7461-24-7.mol

Synonyms:NSC404796;NSC-404796;2,3-Dihydro-1H-inden-1-one semicarbazone

Chemical Property of 2,3-Dihydro-1H-inden-1-one semicarbazone

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• Density: 1.35g/cm³
• XLogP3: 0.9
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 1
• Exact Mass: 189.090211983
• Heavy Atom Count: 14
• Complexity: 262

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CC(=NNC(=O)N)C2=CC=CC=C21
• Isomeric SMILES: C1C/C(=N/NC(=O)N)/C2=CC=CC=C21

Technology Process of 2,3-Dihydro-1H-inden-1-one semicarbazone

There total 4 articles about 2,3-Dihydro-1H-inden-1-one semicarbazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

semicarbazide hydrochloride (563-41-7) + inden-1-one (83-33-0) → Indanon-semicarbazon (7461-24-7)

Guidance literature:

With ethanol; potassium acetate;

Reference yield:

trans-2-iodo-2,3-dihydro-1H-inden-1-ol (90347-62-9) → Indanon-semicarbazon (7461-24-7)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether; KOH

With potassium hydroxide; diethyl ether;

Reference yield:

trans-2-bromo-1-indanol (10368-44-2,78684-69-2) → Indanon-semicarbazon (7461-24-7)

Guidance literature:

Multi-step reaction with 2 steps

1: magnesium bromide etherate

With magnesium bromide ethyl etherate;

upstream raw materials:

semicarbazide hydrochloride

inden-1-one

trans-2-iodo-2,3-dihydro-1H-inden-1-ol

trans-2-bromo-1-indanol