2,6-Dichloro-3-nitrophenol

Base Information

Chemical Name:2,6-Dichloro-3-nitrophenol
CAS No.:28165-61-9
Molecular Formula:C6H3Cl2NO3
Molecular Weight:207.99900
Hs Code.:
DSSTox Substance ID:DTXSID501311665
Nikkaji Number:J88.547I
Mol file:28165-61-9.mol

Synonyms:2,6-Dichloro-3-nitrophenol;28165-61-9;2,6-dichloronitrophenol;SCHEMBL9516342;DTXSID501311665

Suppliers and Price of 2,6-Dichloro-3-nitrophenol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 2,6-Dichloro-3-nitrophenol

Chemical Property:

PSA：66.05000
LogP:3.13040
XLogP3:2.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:0
Exact Mass:206.9489983
Heavy Atom Count:12
Complexity:184

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=C(C(=C1[N+](=O)[O-])Cl)O)Cl

Technology Process of 2,6-Dichloro-3-nitrophenol

There total 1 articles about 2,6-Dichloro-3-nitrophenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 554-84-7
meta-nitrophenol

: 28165-61-9
2,6-dichloro-3-nitrophenol

Guidance literature:: With sulfuryl dichloride; diethylamine; In toluene; at 70 ℃;
DOI:10.1055/s-2004-834924

Reference yield: 91.0%

: 100-39-0
benzyl bromide

: 28165-61-9
2,6-dichloro-3-nitrophenol

: 842117-34-4
1-benzyloxy-2,6-dichloro-3-nitrobenzene

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 16h;
DOI:10.1055/s-2004-834924

Reference yield:

: 28165-61-9
2,6-dichloro-3-nitrophenol

: 842117-36-6
6-benzyloxy-5,7-dichloro-1H-indole

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / Cs₂CO₃ / dimethylformamide / 16 h / 20 °C

2: 57 percent / t-BuOK / dimethylformamide / 0.5 h / -20 - -10 °C

3: 33 percent / H₂ / PtO₂ / ethanol / 2 h / 20 °C / 1551.44 - 1810.02 Torr

With potassium tert-butylate; hydrogen; caesium carbonate; platinum(IV) oxide; In ethanol; N,N-dimethyl-formamide;
DOI:10.1055/s-2004-834924