(5-Chloro-2-methoxyphenyl)acetaldehyde

Base Information

Chemical Name:(5-Chloro-2-methoxyphenyl)acetaldehyde
CAS No.:33567-60-1
Molecular Formula:C₉H₉ClO₂
Molecular Weight:184.622
Hs Code.:
NSC Number:114591
DSSTox Substance ID:DTXSID30297168
Wikidata:Q82038151

Synonyms:33567-60-1;NSC 114591;(5-chloro-2-methoxyphenyl)acetaldehyde;2-(5-chloro-2-methoxyphenyl)acetaldehyde;NSC114591;SCHEMBL929750;DTXSID30297168;AKOS012095429;NSC-114591;EN300-1967294

Suppliers and Price of (5-Chloro-2-methoxyphenyl)acetaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of (5-Chloro-2-methoxyphenyl)acetaldehyde

Chemical Property:

Vapor Pressure:0.00682mmHg at 25°C
Boiling Point:270.5°Cat760mmHg
Flash Point:115.6°C
Density:1.187g/cm³
XLogP3:1.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:184.0291072
Heavy Atom Count:12
Complexity:150

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C(C=C1)Cl)CC=O

Technology Process of (5-Chloro-2-methoxyphenyl)acetaldehyde

There total 4 articles about (5-Chloro-2-methoxyphenyl)acetaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4-Chloro-1-methoxy-2-((E)-2-methoxy-vinyl)-benzene

: 33567-60-1
5-chloro-2-methoxyphenylacetaldehyde

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; water;
DOI:10.1039/c9ob00178f

Reference yield:

: 7035-09-8
5-chloro-2-methoxybenzaldehyde

: 33567-60-1
5-chloro-2-methoxyphenylacetaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / 0 °C

1.2: 0 - 20 °C

2.1: hydrogenchloride / tetrahydrofuran; water

With hydrogenchloride; n-butyllithium; In tetrahydrofuran; hexane; water;
DOI:10.1039/c9ob00178f

Reference yield:

: 635-93-8
5-chlorosalicyclaldehyde

: 33567-60-1
5-chloro-2-methoxyphenylacetaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 48 h / 20 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / 0 °C

2.2: 0 - 20 °C

3.1: hydrogenchloride / tetrahydrofuran; water

With hydrogenchloride; n-butyllithium; potassium carbonate; In tetrahydrofuran; hexane; water; N,N-dimethyl-formamide;
DOI:10.1039/c9ob00178f