5-Chlorosalicylaldehyde

Base Information

Chemical Name:5-Chlorosalicylaldehyde
CAS No.:635-93-8
Molecular Formula:C7H5ClO2
Molecular Weight:156.569
Hs Code.:29130000
European Community (EC) Number:211-244-4
NSC Number:3811
UNII:4GCC8ZKM3O
DSSTox Substance ID:DTXSID7022099
Nikkaji Number:J48.296J
Wikidata:Q27259564
ChEMBL ID:CHEMBL3660361
Mol file:635-93-8.mol

Synonyms:5-chloro-salicylaldehyde

Suppliers and Price of 5-Chlorosalicylaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
5-Chlorosalicyaldehyde
25 g
$ 115.00

TCI Chemical
5-Chlorosalicylaldehyde >98.0%(GC)(T)
5g
$ 13.00

TCI Chemical
5-Chlorosalicylaldehyde >98.0%(GC)(T)
25g
$ 42.00

SynQuest Laboratories
5-Chloro-2-hydroxybenzaldehyde 97%
100 g
$ 79.00

SynQuest Laboratories
5-Chloro-2-hydroxybenzaldehyde 97%
25 g
$ 23.00

Sigma-Aldrich
5-Chlorosalicylaldehyde 98%
5g
$ 31.60

Sigma-Aldrich
5-Chlorosalicylaldehyde 98%
25g
$ 106.00

Matrix Scientific
5-Chloro-2-hydroxybenzaldehyde 95+%
100g
$ 200.00

Matrix Scientific
5-Chloro-2-hydroxybenzaldehyde 95+%
25g
$ 55.00

Matrix Scientific
5-Chloro-2-hydroxybenzaldehyde 95+%
10g
$ 47.00

Total 122 raw suppliers

Chemical Property of 5-Chlorosalicylaldehyde

Chemical Property:

Appearance/Colour:white to very slightly yellow crystalline powder
Vapor Pressure:0.0477mmHg at 25°C
Melting Point:100-102 °C(lit.)
Refractive Index:1.632
Boiling Point:228.8 °C at 760 mmHg
PKA:7.73±0.18(Predicted)
Flash Point:92.2 °C
PSA：37.30000
Density:1.404 g/cm³
LogP:1.85810
Storage Temp.:Keep in dark place,Sealed in dry,Room Temperature
Sensitive.:Air Sensitive
XLogP3:2.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:155.9978071
Heavy Atom Count:10
Complexity:127

Purity/Quality:

99% ^*data from raw suppliers

5-Chlorosalicyaldehyde ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xn,Xi
Hazard Codes:Xi,Xn
Statements: 36/37/38-20/21/22
Safety Statements: 26-36-24/25-36/37/39

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=C(C=C1Cl)C=O)O

Technology Process of 5-Chlorosalicylaldehyde

There total 47 articles about 5-Chlorosalicylaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.4%

: 90-02-8
salicylaldehyde

: 635-93-8
5-chlorosalicyclaldehyde

Guidance literature:: With N-chloro-N-(benzenesulfonyl)benzenesulfonamide; In acetonitrile; at 20 - 25 ℃; for 0.166667h; Green chemistry;
DOI:10.1016/j.tetlet.2020.152689

Reference yield: 83.0%

: 4-chloro-2-(3-(4-chlorophenyl)-1-hydroxyprop-2-yn-1-yl)phenol

: 51118-06-0
1,4-bis(4-chlorophenyl)buta-1,3-diyne

: 635-93-8
5-chlorosalicyclaldehyde

Guidance literature:: With copper(II) acetate monohydrate; In N,N-dimethyl-formamide; at 110 ℃; for 4h;
DOI:10.3184/174751913X13739011239995

Reference yield: 75.0%

: 100-97-0
hexamethylenetetramine

: 106-48-9,82344-39-6
4-chloro-phenol

: 635-93-8
5-chlorosalicyclaldehyde

Guidance literature:: hexamethylenetetramine; 4-chloro-phenol; With trifluoroacetic acid; at 0 - 60 ℃; for 20h;

With sulfuric acid; water; at 20 ℃; for 1h;