3-BROMO-2-NITROTOLUENE

Base Information

Chemical Name:3-BROMO-2-NITROTOLUENE
CAS No.:52414-97-8
Molecular Formula:C7H6BrNO2
Molecular Weight:216.034
Hs Code.:29049090
Mol file:52414-97-8.mol

Synonyms:Toluene,3-bromo-2-nitro- (6CI,7CI);1-Bromo-3-methyl-2-nitrobenzene;2-Nitro-3-bromotoluene;3-Bromo-2-nitrotoluene;6-Bromo-2-methyl-1-nitrobenzene;

Suppliers and Price of 3-BROMO-2-NITROTOLUENE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
3-Bromo-2-nitrotoluene
100mg
$ 60.00

Sigma-Aldrich
3-Bromo-2-nitrotoluene 97%
25g
$ 527.00

Sigma-Aldrich
3-Bromo-2-nitrotoluene 97%
5g
$ 111.00

Matrix Scientific
3-Bromo-2-nitrotoluene 95+%
25g
$ 364.00

Frontier Specialty Chemicals
3-Bromo-2-nitrotoluene 98%
5g
$ 240.00

Frontier Specialty Chemicals
3-Bromo-2-nitrotoluene 98%
1g
$ 60.00

Crysdot
1-Bromo-3-methyl-2-nitrobenzene 95+%
100g
$ 639.00

Chemenu
1-Bromo-3-methyl-2-nitrobenzene 95%
100g
$ 458.00

Chemenu
1-Bromo-3-methyl-2-nitrobenzene 95%
25g
$ 143.00

Biosynth Carbosynth
3-Bromo-2-nitrotoluene
50 g
$ 500.00

Total 39 raw suppliers

Chemical Property of 3-BROMO-2-NITROTOLUENE

Chemical Property:

Appearance/Colour:yellow crystalline low melting mass
Vapor Pressure:0.0689mmHg at 25°C
Melting Point:25-29 °C(lit.)
Refractive Index:1.592
Boiling Point:237.4 °C at 760 mmHg
Flash Point:97.4 °C
PSA：45.82000
Density:1.615g/cm³
LogP:3.18890
Storage Temp.:Sealed in dry,Room Temperature

Purity/Quality:

98% ^*data from raw suppliers

3-Bromo-2-nitrotoluene ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xn
Hazard Codes:Xn
Statements: 36/37/38-20/21/22
Safety Statements: 36/37/39-26-22

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of 3-BROMO-2-NITROTOLUENE

There total 13 articles about 3-BROMO-2-NITROTOLUENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 601-87-6
3-methyl-2-nitroaniline

: 52414-97-8
1-bromo-3-methyl-2-nitro-benzene

Guidance literature:: With tert.-butylnitrite; copper(ll) bromide; In acetonitrile; at 65 ℃; for 0.25h; Heating / reflux;

Reference yield: 57.0%

: 540-80-7
tert.-butylnitrite

: 601-87-6
3-methyl-2-nitroaniline

: 52414-97-8
1-bromo-3-methyl-2-nitro-benzene

Guidance literature:: With copper(I) bromide; In acetonitrile; at 65 ℃; for 0.25h; Heating / reflux;

Reference yield: 40.0%

: 5437-38-7
3-methyl-2-nitrobenzoic acid

: 52414-97-8
1-bromo-3-methyl-2-nitro-benzene

Guidance literature:: With copper(l) iodide; oxygen; copper(I) bromide; In dimethyl sulfoxide; at 160 ℃; for 30h; under 760.051 Torr; Schlenk technique; Sealed tube;
DOI:10.1021/acs.joc.5b02873