3-IODOPHENETOLE

Base Information

• Chemical Name: 3-IODOPHENETOLE
• CAS No.: 29052-00-4
• Molecular Formula: C8H9IO
• Molecular Weight: 248.063
• Mol file: 29052-00-4.mol

Synonyms:3-iodo-phenetole;Phenetole,m-iodo;Aethyl-(3-jod-phenyl)-aether;3-Jodphenetol;Phenetole, m-iodo-;m-Iodophenetol;m-iodo-phenetole;3-Jod-1-aethoxy-benzol;

Chemical Property of 3-IODOPHENETOLE

Chemical Property:

• PSA: 9.23000
• LogP: 2.68990

Purity/Quality:

98%Min ^*data from raw suppliers

1-ETHOXY-3-IODOBENZENE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-IODOPHENETOLE

There total 1 articles about 3-IODOPHENETOLE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.8%

ethyl bromide (74-96-4) + 3-Iodophenol (626-02-8) → 3-ethoxyiodobenzene (29052-00-4)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 90 ℃; for 1h; Inert atmosphere;

DOI:10.1142/S1088424617500389

Reference yield: 71.0%

1H-imidazole (288-32-4) + 3-ethoxyiodobenzene (29052-00-4) → C11H12N2O

Guidance literature:

With copper(I) oxide; caesium carbonate; In N,N-dimethyl-formamide; at 120 ℃; for 12h;

DOI:10.1080/00397911.2017.1353633

Reference yield: 68.5%

3-ethoxyiodobenzene (29052-00-4) → 3-ethoxybenzenethiol (86704-82-7)

Guidance literature:

3-ethoxyiodobenzene; With copper(l) iodide; potassium carbonate; sulfur; In N,N-dimethyl-formamide; at 90 ℃; for 12h; Inert atmosphere;

With sodium tetrahydroborate; In tetrahydrofuran; for 32h; Inert atmosphere;

DOI:10.1142/S1088424617500389

upstream raw materials:

ethyl bromide

3-Iodophenol

Downstream raw materials:

3-ethoxybenzenethiol