2,6-bis(2,4-Dimethylphenyl)-4-Phenylphosphabenzene

Base Information

Chemical Name:2,6-bis(2,4-Dimethylphenyl)-4-Phenylphosphabenzene
CAS No.:293309-69-0
Molecular Formula:C27H25P
Molecular Weight:380.469
Hs Code.:
DSSTox Substance ID:DTXSID00467437
Nikkaji Number:J1.656.690J
Wikidata:Q82294387

Synonyms:2,6-bis(2,4-Dimethylphenyl)-4-Phenylphosphabenzene;293309-69-0;SCHEMBL2309790;DTXSID00467437;YRKKPRNXRCQRIS-UHFFFAOYSA-N

Suppliers and Price of 2,6-bis(2,4-Dimethylphenyl)-4-Phenylphosphabenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,6-bis(2,4-Dimethylphenyl)-4-Phenylphosphabenzene

Chemical Property:

XLogP3:5.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:3
Exact Mass:380.169387795
Heavy Atom Count:28
Complexity:447

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=C(C=C1)C2=CC(=CC(=P2)C3=C(C=C(C=C3)C)C)C4=CC=CC=C4)C

Technology Process of 2,6-bis(2,4-Dimethylphenyl)-4-Phenylphosphabenzene

There total 4 articles about 2,6-bis(2,4-Dimethylphenyl)-4-Phenylphosphabenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 2,6-Bis(2,4-dimethylphenyl)-4-phenylpyrylium tetrafluoroborate

: 293309-69-0
bis-2,6-(2,4-dimethylphenyl)-4-phenylphosphabenzene

Guidance literature:: With Tris(trimethylsilyl)phosphane; phosphan; In butan-1-ol; at 110 ℃; for 4h; under 22501.8 Torr;
DOI:10.1002/1521-3765(20010716)7:14<3106::AID-CHEM3106>3.0.CO;2-Y

Reference yield:

: 100-52-7
benzaldehyde

: 293309-69-0
bis-2,6-(2,4-dimethylphenyl)-4-phenylphosphabenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 32 percent / diethyl ether; 1,2-dichloro-ethane / 4 h / 80 °C

2: 53 percent / P(TMS)3; PH₃ / butan-1-ol / 4 h / 110 °C / 22501.8 Torr

With Tris(trimethylsilyl)phosphane; phosphan; In diethyl ether; 1,2-dichloro-ethane; butan-1-ol;
DOI:10.1002/1521-3765(20010716)7:14<3106::AID-CHEM3106>3.0.CO;2-Y

Reference yield:

: 89-74-7
2,4-dimethylacetophenone.

: 293309-69-0
bis-2,6-(2,4-dimethylphenyl)-4-phenylphosphabenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 32 percent / diethyl ether; 1,2-dichloro-ethane / 4 h / 80 °C

2: 53 percent / P(TMS)3; PH₃ / butan-1-ol / 4 h / 110 °C / 22501.8 Torr

With Tris(trimethylsilyl)phosphane; phosphan; In diethyl ether; 1,2-dichloro-ethane; butan-1-ol;
DOI:10.1002/1521-3765(20010716)7:14<3106::AID-CHEM3106>3.0.CO;2-Y