2-[3-[(4-chlorophenyl)methyl]-2-methyl-5-nitro-imidazol-4-yl]sulfanyla cetamide

Base Information

Chemical Name:2-[3-[(4-chlorophenyl)methyl]-2-methyl-5-nitro-imidazol-4-yl]sulfanyla cetamide
CAS No.:77952-76-2
Molecular Formula:C₁₃H₁₃ClN₄O₃S
Molecular Weight:340.79
Hs Code.:2933290090
Mol file:77952-76-2.mol

Synonyms:2-[3-[(4-chlorophenyl)methyl]-2-methyl-5-nitro-imidazol-4-yl]sulfanyla cetamide

Suppliers and Price of 2-[3-[(4-chlorophenyl)methyl]-2-methyl-5-nitro-imidazol-4-yl]sulfanyla cetamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 2-[3-[(4-chlorophenyl)methyl]-2-methyl-5-nitro-imidazol-4-yl]sulfanyla cetamide

Chemical Property:

Vapor Pressure:1.76E-13mmHg at 25°C
Boiling Point:580.8°C at 760 mmHg
Flash Point:305°C
PSA：133.02000
Density:1.52g/cm³
LogP:4.05170

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-[3-[(4-chlorophenyl)methyl]-2-methyl-5-nitro-imidazol-4-yl]sulfanyla cetamide

There total 2 articles about 2-[3-[(4-chlorophenyl)methyl]-2-methyl-5-nitro-imidazol-4-yl]sulfanyla cetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 77952-63-7
3-(4-Chloro-benzyl)-2-methyl-5-nitro-3H-imidazole-4-thiol; compound with ammonia

: 79-07-2
Chloroacetamide

: 77952-76-2
2-[3-(4-Chloro-benzyl)-2-methyl-5-nitro-3H-imidazol-4-ylsulfanyl]-acetamide

Guidance literature:: In methanol; water; Heating; 1.) reflux, 6-7 h, 2.) overnight;
DOI:10.1007/BF01149151

Reference yield:

: 68019-73-8
5-bromo-1-(4-chloro-benzyl)-2-methyl-4-nitro-1H-imidazole

: 77952-76-2
2-[3-(4-Chloro-benzyl)-2-methyl-5-nitro-3H-imidazol-4-ylsulfanyl]-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / H₂S, ethanolic NH₃ / dimethylformamide / 0.17 h

2: 65 percent / methanol; H₂O / Heating; 1.) reflux, 6-7 h, 2.) overnight

With hydrogen sulfide; ammonia; In methanol; water; N,N-dimethyl-formamide;
DOI:10.1007/BF01149151