2,5-Cyclohexadien-1-one, 4-methyl-4-(trichloromethyl)-, [4-methyl-4-(trichloromethyl)-2,5-cyclohexadien-1-ylidene]hydrazone

Base Information

• Chemical Name: 2,5-Cyclohexadien-1-one, 4-methyl-4-(trichloromethyl)-, [4-methyl-4-(trichloromethyl)-2,5-cyclohexadien-1-ylidene]hydrazone
• CAS No.: 2943-18-2
• Molecular Formula: C₁₆H₁₄Cl₆N₂
• Molecular Weight: 447.019
• Mol file: 2943-18-2.mol

Synonyms:

Chemical Property of 2,5-Cyclohexadien-1-one, 4-methyl-4-(trichloromethyl)-, [4-methyl-4-(trichloromethyl)-2,5-cyclohexadien-1-ylidene]hydrazone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 2,5-Cyclohexadien-1-one, 4-methyl-4-(trichloromethyl)-, [4-methyl-4-(trichloromethyl)-2,5-cyclohexadien-1-ylidene]hydrazone

There total 2 articles about 2,5-Cyclohexadien-1-one, 4-methyl-4-(trichloromethyl)-, [4-methyl-4-(trichloromethyl)-2,5-cyclohexadien-1-ylidene]hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.3%

3,6-dibromo-phenanthrene-9,10-dione (53348-05-3) + 4-methyl-4-trichloromethylcyclohexa-2,5-dienone hydrazone → N,N'-Bis-(4-methyl-4-trichloromethyl-cyclohexa-2,5-dienylidene)-hydrazine (2943-18-2) + 3,6-Dibromo-10-(p-tolyl-hydrazono)-10H-phenanthren-9-one

Guidance literature:

In ethanol; dimethyl sulfoxide; at 100 - 110 ℃; for 5h;

DOI:10.1007/BF02494379

Reference yield:

4-methyl-4-(trichloromethyl)cyclohexa-2,5-dien-1-one (3274-12-2) → N,N'-Bis-(4-methyl-4-trichloromethyl-cyclohexa-2,5-dienylidene)-hydrazine (2943-18-2)

Guidance literature:

With hydrazine hydrate; In ethanol; at 70 ℃; for 5h;

DOI:10.1007/BF02496230

upstream raw materials:

3,6-dibromo-phenanthrene-9,10-dione

4-methyl-4-(trichloromethyl)cyclohexa-2,5-dien-1-one