1-(3-Hydroxy-3-methylbut-1-ynyl)cyclohexanol

Base Information

Chemical Name:1-(3-Hydroxy-3-methylbut-1-ynyl)cyclohexanol
CAS No.:2960-28-3
Molecular Formula:C11H18O2
Molecular Weight:182.263
Hs Code.:
DSSTox Substance ID:DTXSID00444309
Nikkaji Number:J706.284B
Wikidata:Q82262419
Mol file:2960-28-3.mol

Synonyms:2960-28-3;1-(3-hydroxy-3-methylbut-1-ynyl)cyclohexanol;SCHEMBL3661461;DTXSID00444309;KSLANYYODUTZEF-UHFFFAOYSA-N;1-(3-Hydroxy-3-methyl-1-butynyl)cyclohexan-1-ol

Suppliers and Price of 1-(3-Hydroxy-3-methylbut-1-ynyl)cyclohexanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 1-(3-Hydroxy-3-methylbut-1-ynyl)cyclohexanol

Chemical Property:

XLogP3:1.1
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:182.130679813
Heavy Atom Count:13
Complexity:235

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C#CC1(CCCCC1)O)O

Technology Process of 1-(3-Hydroxy-3-methylbut-1-ynyl)cyclohexanol

There total 3 articles about 1-(3-Hydroxy-3-methylbut-1-ynyl)cyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: lithium 4-lithio-2-methyl-3-butyn-2-olate

: 2960-28-3
1-hydroxy-1-(3-hydroxy-3-methyl-1-butynyl)cyclohexane

Guidance literature:: In tetrahydrofuran; at 20 - 23 ℃;
DOI:10.1023/A:1021691426904

Reference yield:

: 78-27-3
1-Ethynylcyclohexan-1-ol

: 67-64-1
acetone

: 2960-28-3
1-hydroxy-1-(3-hydroxy-3-methyl-1-butynyl)cyclohexane

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1.) THF, hexane, -78 deg C, 2 h, 2.) THF, hexane, -65 deg C, 6 h;
DOI:10.1246/bcsj.56.3078