4-Formylmonomethylaminoazobenzene

Base Information

• Chemical Name: 4-Formylmonomethylaminoazobenzene
• CAS No.: 4845-14-1
• Molecular Formula: C14H13N3O
• Molecular Weight: 239.277
• DSSTox Substance ID: DTXSID001039933
• Nikkaji Number: J33.844C
• Mol file: 4845-14-1.mol

Synonyms:4-Formylmonomethylaminoazobenzene;4845-14-1;N-Formyl-N-methyl-p-(phenylazo)aniline;ANILINE, N-FORMYL-N-METHYL-p-(PHENYLAZO)-;SCHEMBL14156423;DTXSID001039933;Formanilide, N-methyl-4'-(phenylazo)-;LS-19824;N-Methyl-N-[4-(phenylazo)phenyl]formamide;Formamide, N-methyl-N-[4-(phenylazo)phenyl]-;Formamide, N-methyl-N-[4-(2-phenyldiazenyl)phenyl]-

Chemical Property of 4-Formylmonomethylaminoazobenzene

Chemical Property:

• Vapor Pressure: 1.15E-07mmHg at 25°C
• Refractive Index: 1.5700 (estimate)
• Boiling Point: 431.9°Cat760mmHg
• PKA: -1.04±0.50(Predicted)
• Flash Point: 215°C
• PSA: 45.03000
• Density: 1.09g/cm³
• LogP: 4.33050
• XLogP3: 2.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 3
• Exact Mass: 239.105862047
• Heavy Atom Count: 18
• Complexity: 279

Purity/Quality:

99% ^*data from raw suppliers

N-FORMYL-N-METHYL-PARA-(PHENYLAZO)ANILINE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C=O)C1=CC=C(C=C1)N=NC2=CC=CC=C2

Technology Process of 4-Formylmonomethylaminoazobenzene

There total 6 articles about 4-Formylmonomethylaminoazobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

4-(phenylazo)-N,N-dimethylaniline amino oxide (2747-31-1) → formic acid-(N-methyl-4-phenylazo-anilide) (4845-14-1) + N-methyl-4-aminoazobenzene (621-90-9) + methyl yellow (60-11-7)

Guidance literature:

In benzene; at 17 ℃; for 6h; Irradiation;

Reference yield: 75.0%

4-(phenyl-ONN-azoxy)-N,N-dimethylaniline (13921-71-6) → formic acid-(N-methyl-4-phenylazo-anilide) (4845-14-1) + 4-Dimethylamino-2-hydroxy-azobenzol (63020-88-2) + p-dimethylaminonitrosobenzene (138-89-6)

Guidance literature:

In benzene; for 7h; Irradiation;

DOI:10.1021/jo00351a018

Reference yield: 13.0%

4-(phenyl-ONN-azoxy)-N,N-dimethylaniline amino oxide (13921-67-0) → formic acid-(N-methyl-4-phenylazo-anilide) (4845-14-1) + N-methyl-4-aminoazobenzene (621-90-9) + methyl yellow (60-11-7) + 4-(phenyl-ONN-azoxy)-N,N-dimethylaniline (13921-71-6)

Guidance literature:

In benzene; at 17 ℃; for 6h; Irradiation;

upstream raw materials:

formic acid

N-methyl-4-aminoazobenzene

4-(phenylazo)-N,N-dimethylaniline amino oxide

4-(phenyl-ONN-azoxy)-N,N-dimethylaniline amino oxide

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