2-Propenoic acid, 2-methyl-, 2-(ethylphenylamino)ethyl ester

Base Information

• Chemical Name: 2-Propenoic acid, 2-methyl-, 2-(ethylphenylamino)ethyl ester
• CAS No.: 2997-87-7
• Molecular Formula: C14H19NO2
• Molecular Weight: 233.31
• European Community (EC) Number: 608-435-3
• DSSTox Substance ID: DTXSID30482850
• Nikkaji Number: J799.934H
• Wikidata: Q82319667
• Mol file: 2997-87-7.mol

Synonyms:2-Propenoic acid, 2-methyl-, 2-(ethylphenylamino)ethyl ester;2997-87-7;SCHEMBL554904;DTXSID30482850;WTBIHKZYDZQMQA-UHFFFAOYSA-N;2-(ethyl(phenyl)amino)ethyl methacrylate;2-[ethyl(phenyl)amino]ethyl 2-methylprop-2-enoate

Chemical Property of 2-Propenoic acid, 2-methyl-, 2-(ethylphenylamino)ethyl ester

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• XLogP3: 3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 7
• Exact Mass: 233.141578849
• Heavy Atom Count: 17
• Complexity: 257

Purity/Quality:

99.90% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCN(CCOC(=O)C(=C)C)C1=CC=CC=C1

Technology Process of 2-Propenoic acid, 2-methyl-, 2-(ethylphenylamino)ethyl ester

There total 5 articles about 2-Propenoic acid, 2-methyl-, 2-(ethylphenylamino)ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2-( N-ethylanilino)ethanol (92-50-2) + methacrylic acid methyl ester (80-62-6,114512-63-9,143476-91-9,25188-98-1,9011-14-7) → N-ethyl-N-(2-methacryloyloxyethyl)aniline (2997-87-7)

Guidance literature:

With potassium phosphate; 4-methoxy-phenol; at 70 ℃; under 225.023 Torr;

Reference yield: 86.0%

2-( N-ethylanilino)ethanol (92-50-2) + Methacryloyl chloride (920-46-7,26937-45-1) → N-ethyl-N-(2-methacryloyloxyethyl)aniline (2997-87-7)

Guidance literature:

With triethylamine; In dichloromethane; for 3h; Cooling with ice;

DOI:10.1039/c4tc00996g

Reference yield:

2-( N-ethylanilino)ethanol (92-50-2) + dioctyltin(IV) oxide (870-08-6) + methacrylic acid methyl ester (80-62-6,114512-63-9,143476-91-9,25188-98-1,9011-14-7) → N-ethyl-N-(2-methacryloyloxyethyl)aniline (2997-87-7)

Guidance literature:

In dichloromethane; toluene;

upstream raw materials:

2-( N-ethylanilino)ethanol

methacrylic acid methyl ester

dioctyltin(IV) oxide

Methacryloyl chloride

Downstream raw materials:

4-[4'-(N,N-methacryloyloxy-2-ethyl-ethylamino)phenyl]-3-nitro-benzoic acid