Acridine, tetradecahydro-10-phenyl-

Base Information

• Chemical Name: Acridine, tetradecahydro-10-phenyl-
• CAS No.: 30426-05-2
• Molecular Formula: C19H27N
• Molecular Weight: 269.43
• Mol file: 30426-05-2.mol

Synonyms:

Chemical Property of Acridine, tetradecahydro-10-phenyl-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Acridine, tetradecahydro-10-phenyl-

There total 5 articles about Acridine, tetradecahydro-10-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

2-hydroxytricyclo[7.3.1.02,7]tridecan-13-one (2544-00-5,20557-98-6) + aniline (62-53-3) → N-phenylperhydroacridine (30426-05-2) + 2,13-dihydroxytricyclo<7.3.1.02.7>tridecane (1624-21-1,20557-99-7,20558-00-3)

Guidance literature:

With hydrogen; nickel ruthenium; at 100 ℃; under 75230.9 Torr;

Reference yield: 50.0%

aniline (62-53-3) + bis(2-oxocyclohexyl)methane (3137-39-1) → N-phenylperhydroacridine (30426-05-2)

Guidance literature:

With hydrogen; nickel ruthenium; In methanol; at 100 ℃; under 7598.1 Torr; Product distribution; other catalyst;

DOI:10.1007/BF00568950

Reference yield:

10-phenyl-sym-octahydroacridinium perchlorate → cis-syn-cis-10-phenylperhydroacridine (114544-16-0) + cis-anti-cis-10-phenylperhydroacridine (30382-37-7,30426-05-2,42885-32-5,114544-13-7,114544-16-0)

Guidance literature:

With hydrogen; aniline; nickel ruthenium; In ethanol; at 100 ℃; under 75006 Torr; Title compound not separated from byproducts;

DOI:10.1007/BF02256983

upstream raw materials:

2-hydroxytricyclo[7.3.1.0^2,7]tridecan-13-one

aniline

bis(2-oxocyclohexyl)methane

nitrobenzene

Refernces

• 1、 Nikolaeva, T. G.,Yudovich, L. M.,Komyagin, N. T.,Yanovskii, A. I.,Struchkov, Yu. T.,Kriven'ko, A. P.. "SATURATED NITROGEN-CONTAINING HETEROCYCLES. 16. CATALYTIC SYNTHESIS OF N-ARYLPERHYDROACRIDINES". . p. 932 - 937. Retrieved 2007/10/02.
• 2、 Kriven'ko, A. P.,Nikolaeva, T. G.,Yudovich, L. M.,Komyagin, N. T.,Yanovskii, A. I.,et al.. "SATURATED NITROGEN-CONTAINING HETEROCYCLES. 13. PERHYDROACRIDINES. SYNTHESIS AND STEREOCHEMISTRY". . p. 1324 - 1329. Retrieved 2007/10/02.