Diethyl 4,4'-oxydibenzoate

Base Information

Chemical Name:Diethyl 4,4'-oxydibenzoate
CAS No.:3096-86-4
Molecular Formula:C18H18O5
Molecular Weight:314.338
Hs Code.:
DSSTox Substance ID:DTXSID00575642
Wikidata:Q82465052
Mol file:3096-86-4.mol

Synonyms:4-ethoxycarbonylphenyl ether;Diethyl 4,4'-oxydibenzoate;3096-86-4;SCHEMBL8656770;DTXSID00575642

Suppliers and Price of Diethyl 4,4'-oxydibenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of Diethyl 4,4'-oxydibenzoate

Chemical Property:

XLogP3:3.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:8
Exact Mass:314.11542367
Heavy Atom Count:23
Complexity:343

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C1=CC=C(C=C1)OC2=CC=C(C=C2)C(=O)OCC

Technology Process of Diethyl 4,4'-oxydibenzoate

There total 3 articles about Diethyl 4,4'-oxydibenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 586-76-5
4-Bromobenzoic acid

: 3096-86-4
4,4'-oxybis(ethyl benzoate)

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid / 4 h / Reflux

2: copper(l) iodide; dimethylaminoacetic acid; caesium carbonate / 1,4-dioxane / 24 h / Reflux; Inert atmosphere

With copper(l) iodide; dimethylaminoacetic acid; sulfuric acid; caesium carbonate; In 1,4-dioxane; 2: Ullmann condensation;
DOI:10.1007/s12272-010-1205-2

Reference yield:

: 99-96-7
4-hydroxy-benzoic acid

: 3096-86-4
4,4'-oxybis(ethyl benzoate)

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid / 5 h / Reflux

2: copper(l) iodide; dimethylaminoacetic acid; caesium carbonate / 1,4-dioxane / 24 h / Reflux; Inert atmosphere

With copper(l) iodide; dimethylaminoacetic acid; sulfuric acid; caesium carbonate; In 1,4-dioxane; 2: Ullmann condensation;
DOI:10.1007/s12272-010-1205-2

Reference yield:

: 120-47-8
Ethyl 4-hydroxybenzoate

: 5798-75-4
Ethyl 4-bromobenzoate

: 3096-86-4
4,4'-oxybis(ethyl benzoate)

Guidance literature:: With copper(l) iodide; dimethylaminoacetic acid; caesium carbonate; In 1,4-dioxane; for 24h; Reflux; Inert atmosphere;
DOI:10.1007/s12272-010-1205-2