Benzoic acid, 2-hydroxy-6-(2-propenyl)-

Base Information

Chemical Name:Benzoic acid, 2-hydroxy-6-(2-propenyl)-
CAS No.:312962-10-0
Molecular Formula:C10H10O3
Molecular Weight:178.188
Hs Code.:
DSSTox Substance ID:DTXSID70462939
Nikkaji Number:J1.487.007E
Wikidata:Q82287591
Mol file:312962-10-0.mol

Synonyms:Benzoic acid, 2-hydroxy-6-(2-propenyl)-;312962-10-0;SCHEMBL3803126;DTXSID70462939

Suppliers and Price of Benzoic acid, 2-hydroxy-6-(2-propenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzoic acid, 2-hydroxy-6-(2-propenyl)-

Chemical Property:

XLogP3:2.7
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:178.062994177
Heavy Atom Count:13
Complexity:200

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C=CCC1=C(C(=CC=C1)O)C(=O)O

Technology Process of Benzoic acid, 2-hydroxy-6-(2-propenyl)-

There total 5 articles about Benzoic acid, 2-hydroxy-6-(2-propenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 204846-40-2
2,2-dimethyl-5-(2-propenyl)-4H-1,3-benzodioxin-4-one

: 312962-10-0
2-allyl-6-hydroxy-benzoic acid

Guidance literature:: With potassium hydroxide; In tetrahydrofuran; at 65 ℃; for 12h;
DOI:10.1021/ol015822v

Reference yield: 90.0%

: 325172-28-9
2-allyl-6-methoxy-benzoic acid

: 312962-10-0
2-allyl-6-hydroxy-benzoic acid

Guidance literature:: With boron trichloride; tetra-(n-butyl)ammonium iodide; In dichloromethane; at -78 - 20 ℃;
DOI:10.1021/jo0301550

Reference yield:

: 154714-19-9
5-hydroxy-2,2-dimethyl-4H-benzo[d][1,3]dioxin-4-one

: 312962-10-0
2-allyl-6-hydroxy-benzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / pyridine

2: 83 percent / KOMe / [PdCl₂(dppf)] / tetrahydrofuran

3: 96 percent / BCl₃ / CH₂Cl₂ / 5 h / 20 °C

With pyridine; potassium methanolate; boron trichloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; dichloromethane;
DOI:10.1002/1521-3765(20011217)7:24<5286::AID-CHEM5286>3.0.CO;2-G