2-allyl-6-hydroxybenzoic acid 1-(2-allyloxyethyl)-3-(4-methoxybenzyloxy)propyl ester

Base Information

Chemical Name:2-allyl-6-hydroxybenzoic acid 1-(2-allyloxyethyl)-3-(4-methoxybenzyloxy)propyl ester
CAS No.:794588-46-8
Molecular Formula:C₂₆H₃₂O₆
Molecular Weight:440.536
Hs Code.:

Synonyms:2-allyl-6-hydroxybenzoic acid 1-(2-allyloxyethyl)-3-(4-methoxybenzyloxy)propyl ester

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Chemical Property of 2-allyl-6-hydroxybenzoic acid 1-(2-allyloxyethyl)-3-(4-methoxybenzyloxy)propyl ester

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Technology Process of 2-allyl-6-hydroxybenzoic acid 1-(2-allyloxyethyl)-3-(4-methoxybenzyloxy)propyl ester

There total 2 articles about 2-allyl-6-hydroxybenzoic acid 1-(2-allyloxyethyl)-3-(4-methoxybenzyloxy)propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 312962-10-0
2-allyl-6-hydroxy-benzoic acid

: 794588-45-7
1-allyloxy-5-(4-methoxybenzyloxy)pentan-3-ol

: 794588-46-8
2-allyl-6-hydroxybenzoic acid 1-(2-allyloxyethyl)-3-(4-methoxybenzyloxy)propyl ester

Guidance literature:: 2-allyl-6-hydroxy-benzoic acid; 1-allyloxy-5-(4-methoxybenzyloxy)pentan-3-ol; With di-isopropyl azodicarboxylate; triphenylphosphine; In diethyl ether; at 0 - 20 ℃;

With potassium carbonate; In methanol; Further stages.;
DOI:10.1016/j.tet.2004.06.146

Reference yield:

: 794588-83-3
(S)-3-(tert-butyldimethylsilyloxy)-5-(4-methoxybenzyloxy)pentan-1-ol

: 794588-46-8
2-allyl-6-hydroxybenzoic acid 1-(2-allyloxyethyl)-3-(4-methoxybenzyloxy)propyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: 78 percent / NaH / tetrahydrofuran / 20 h / 20 °C

2.1: 74 percent / TBAF / tetrahydrofuran / 5 h / 20 °C

3.1: diisopropyl azodicarboxylate; PPh₃ / diethyl ether / 0 - 20 °C

3.2: 96 percent / K₂CO₃ / methanol

With di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; sodium hydride; triphenylphosphine; In tetrahydrofuran; diethyl ether; 3.1: Mitsunobu reaction;
DOI:10.1016/j.tet.2004.06.146