Phosphinic chloride, (2-chloroethenyl)phenyl-

Base Information

• Chemical Name: Phosphinic chloride, (2-chloroethenyl)phenyl-
• CAS No.: 3135-58-8
• Molecular Formula: C8H7Cl2OP
• Molecular Weight: 221.023
• Mol file: 3135-58-8.mol

Synonyms:

Chemical Property of Phosphinic chloride, (2-chloroethenyl)phenyl-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Phosphinic chloride, (2-chloroethenyl)phenyl-

There total 8 articles about Phosphinic chloride, (2-chloroethenyl)phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

-butyl vinyl ether (111-34-2,92680-80-3) + phenyltetrachlorophosphorane (4895-65-2) → phenyl-β-chlorovinylphosphinic chloride (3135-58-8)

Guidance literature:

In benzene; for 24h;

Reference yield:

phenyltetrachlorophosphorane (4895-65-2) → phenyl-β-chlorovinylphosphinic chloride (3135-58-8) + phenyl-β-ethoxyvinylphosphinic chloride (90876-11-2) + Dichlorophenylphosphine (644-97-3)

Guidance literature:

With phosphan; ethyl vinyl ether; Yield given. Multistep reaction. Yields of byproduct given;

Reference yield:

phenyltetrachlorophosphorane (4895-65-2) + ethyl vinyl ether (109-92-2,25104-37-4) → phenyl-β-chlorovinylphosphinic chloride (3135-58-8) + phenyl-β-ethoxyvinylphosphinic chloride (90876-11-2) + Dichlorophenylphosphine (644-97-3)

Guidance literature:

With phosphan; Yield given. Multistep reaction. Yields of byproduct given;

upstream raw materials:

-butyl vinyl ether

phenyltetrachlorophosphorane

ethyl vinyl ether

Dichlorophenylphosphine

Refernces

• 1、 Kormachev, V. V.,Mitrasov, Yu. N.,Kornilov, A. G.. "PHOSPHORUS-CONTAINING INTERMEDIATES AND DYES. VIII. SYNTHESIS OF PHOSPHINIC DERIVATIVES IN REACTIONS OF ORGANOTETRACHLOROPHOSPHORANES WITH VINYL ETHERS". . p. 679 - 683. Retrieved 2007/10/02.