3H-Pyrazole-3-thione, 2,4-dihydro-5-methyl-2-phenyl-4-[(8-quinolinylamino)methylene]-, (4Z)-

Base Information

Chemical Name:3H-Pyrazole-3-thione, 2,4-dihydro-5-methyl-2-phenyl-4-[(8-quinolinylamino)methylene]-, (4Z)-
CAS No.:313945-31-2
Molecular Formula:C₂₀H₁₆N₄S
Molecular Weight:344.44
Hs Code.:
Mol file:313945-31-2.mol

Synonyms:5-Methyl-2-phenyl-4-[1-(quinolin-8-ylamino)-meth-(Z)-ylidene]-2,4-dihydro-pyrazole-3-thione;

Suppliers and Price of 3H-Pyrazole-3-thione, 2,4-dihydro-5-methyl-2-phenyl-4-[(8-quinolinylamino)methylene]-, (4Z)-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3H-Pyrazole-3-thione, 2,4-dihydro-5-methyl-2-phenyl-4-[(8-quinolinylamino)methylene]-, (4Z)-

Chemical Property:

PSA：72.61000
LogP:4.32770

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3H-Pyrazole-3-thione, 2,4-dihydro-5-methyl-2-phenyl-4-[(8-quinolinylamino)methylene]-, (4Z)-

There total 1 articles about 3H-Pyrazole-3-thione, 2,4-dihydro-5-methyl-2-phenyl-4-[(8-quinolinylamino)methylene]-, (4Z)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 578-66-5
8-amino quinoline

: 24628-79-3
1-phenyl-3-methyl-5-sulfanyl-pyrazole-4-carbaldehyde

: 313945-31-2
(4Z)-5-methyl-2-phenyl-4-[(quinolin-8-ylimino)methyl]-2,4-dihydro-3H-pyrazol-3-thione

Guidance literature:: In ethanol;
DOI:10.1007/BF02494925

Reference yield: 71.0%

: 557-34-6
zinc diacetate

: 313945-31-2
(4Z)-5-methyl-2-phenyl-4-[(quinolin-8-ylimino)methyl]-2,4-dihydro-3H-pyrazol-3-thione

: bis[3-methyl-1-phenyl-4-[(E)-(quinolin-8-ylimino)methyl]-1H-pyrazole-5-thiolato]zinc(II)

Guidance literature:: In methanol; reflux of methanolic soln. of C9H6N(NCH)C3N2(SH)(Ph)(Me) (2 equiv.) and Zn(CH3COO)2 for 30-40 min; pptn., filtration, washing with ethanol, recrystn. from mixt. of CH2Cl2 and hexane; elem. anal.;
DOI:10.1007/s11172-005-0298-z

Reference yield: 65.0%

: 543-90-8
cadmium(II) acetate

: 313945-31-2
(4Z)-5-methyl-2-phenyl-4-[(quinolin-8-ylimino)methyl]-2,4-dihydro-3H-pyrazol-3-thione

: bis[3-methyl-1-phenyl-4-[(E)-(quinolin-8-ylimino)methyl]-1H-pyrazole-5-thiolato]cadmium(II)

Guidance literature:: In methanol; reflux of methanolic soln. of C9H6N(NCH)C3N2(SH)(Ph)(Me) (2 equiv.) and Cd(CH3COO)2 for 30-40 min; pptn., filtration, washing with ethanol, recrystn. from mixt. of CH2Cl2 and hexane;
DOI:10.1007/s11172-005-0298-z