2-[4-(azocan-1-yl)but-2-ynyl]isoindole-1,3-dione

Base Information

Chemical Name:2-[4-(azocan-1-yl)but-2-ynyl]isoindole-1,3-dione
CAS No.:19446-30-1
Molecular Formula:C₁₉H₂₂N₂O₂
Molecular Weight:310.396
Hs Code.:2933990090
Mol file:19446-30-1.mol

Synonyms:1H-Isoindole-1,3(2H)-dione,2-[4-(hexahydro-1(2H)-azocinyl)-2-butynyl]- (9CI); Phthalimide,N-[4-(hexahydro-1(2H)-azocinyl)-2-butynyl]- (8CI); Azocine,1H-isoindole-1,3(2H)-dione deriv.

Suppliers and Price of 2-[4-(azocan-1-yl)but-2-ynyl]isoindole-1,3-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2-[4-(azocan-1-yl)but-2-ynyl]isoindole-1,3-dione

Chemical Property:

Vapor Pressure:9.8E-09mmHg at 25°C
Boiling Point:462.5°Cat760mmHg
Flash Point:198.2°C
PSA：40.62000
Density:1.169g/cm³
LogP:2.42790

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-[4-(azocan-1-yl)but-2-ynyl]isoindole-1,3-dione

There total 1 articles about 2-[4-(azocan-1-yl)but-2-ynyl]isoindole-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1121-92-2
heptamethyleneimine

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 7223-50-9
N-propargylphthalimide

: 19446-30-1
2-(4-Azocan-1-yl-but-2-ynyl)-isoindole-1,3-dione

Guidance literature:: With copper(l) chloride; In 1,4-dioxane; for 1h; Heating;

Reference yield: 40.0%

: 19446-30-1
2-(4-Azocan-1-yl-but-2-ynyl)-isoindole-1,3-dione

: 81639-05-6
4-Azocan-1-yl-but-2-ynylamine

: 81639-02-3
N¹,N²-bis-[4-(perhydro-1-azapinyl)-2-butynyl]phthalamide

Guidance literature:: With hydrazine hydrate; In ethanol; for 1.5h; Heating;

Reference yield:

: 19446-30-1
2-(4-Azocan-1-yl-but-2-ynyl)-isoindole-1,3-dione

: 81639-00-1
(S)-5-Oxo-pyrrolidine-2-carboxylic acid (4-azocan-1-yl-but-2-ynyl)-amide

Guidance literature:: Multi-step reaction with 2 steps

1: 43 percent / hydrazine hydrate / ethanol / 1.5 h / Heating

2: 48 percent / dimethylformamide / 16 h / Ambient temperature

With hydrazine hydrate; In ethanol; N,N-dimethyl-formamide;