5,5-Dimethyl-3-phenyl-2-cyclohexen-1-ol

Base Information

Chemical Name:5,5-Dimethyl-3-phenyl-2-cyclohexen-1-ol
CAS No.:31952-17-7
Molecular Formula:C14H18O
Molecular Weight:202.296
Hs Code.:
DSSTox Substance ID:DTXSID801280495
Nikkaji Number:J2.283.311A

Synonyms:DTXSID801280495;AKOS014508810;31952-17-7;5,5-Dimethyl-3-phenyl-2-cyclohexen-1-ol

Suppliers and Price of 5,5-Dimethyl-3-phenyl-2-cyclohexen-1-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5,5-Dimethyl-3-phenyl-2-cyclohexen-1-ol

Chemical Property:

XLogP3:3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:202.135765193
Heavy Atom Count:15
Complexity:246

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1(CC(C=C(C1)C2=CC=CC=C2)O)C

Technology Process of 5,5-Dimethyl-3-phenyl-2-cyclohexen-1-ol

There total 4 articles about 5,5-Dimethyl-3-phenyl-2-cyclohexen-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 135879-26-4
3,3-Dimethyl-5-hexyn-1-al

: 98-80-6
phenylboronic acid

: 31952-17-7
5,5-dimethyl-3,4,5,6-tetrahydro-[1,1'-biphenyl]-3-ol

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In methanol; at 65 ℃; for 12h;
DOI:10.1021/ja056458o

Reference yield:

: 36047-17-3
5,5-dimethyl-3-phenyl-2-cyclohexen-1-one

: 31952-17-7
5,5-dimethyl-3,4,5,6-tetrahydro-[1,1'-biphenyl]-3-ol

Guidance literature:: With sodium hydroxide; sodium tetrahydroborate; In 1,4-dioxane; water; at 24.9 ℃; Rate constant;
DOI:10.1039/P29860001327

Reference yield:

: 126-81-8
dimedone

: 31952-17-7
5,5-dimethyl-3,4,5,6-tetrahydro-[1,1'-biphenyl]-3-ol

Guidance literature:: Multi-step reaction with 3 steps

1: iodine / 20 °C

2: tetrahydrofuran / 0 - 20 °C / Inert atmosphere

3: methanol; sodium tetrahydroborate / 0.08 h / 0 °C / Inert atmosphere

With methanol; sodium tetrahydroborate; iodine; In tetrahydrofuran;
DOI:10.1002/anie.201911730