5,5-Dimethyl-3-phenyl-2-cyclohexen-1-one

Base Information

Chemical Name:5,5-Dimethyl-3-phenyl-2-cyclohexen-1-one
CAS No.:36047-17-3
Molecular Formula:C14H16O
Molecular Weight:200.28
Hs Code.:
DSSTox Substance ID:DTXSID20189604
Nikkaji Number:J1.650.642G
Wikidata:Q83061762

Synonyms:5,5-Dimethyl-3-phenyl-2-cyclohexen-1-one;5,5-dimethyl-3-phenylcyclohex-2-en-1-one;36047-17-3;SCHEMBL8007243;DTXSID20189604;STK082115;AKOS005392500;CCG-288776;5,5-Dimethyl-3-phenylcyclohex-2-enone

Suppliers and Price of 5,5-Dimethyl-3-phenyl-2-cyclohexen-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 5,5-Dimethyl-3-phenyl-2-cyclohexen-1-one

Chemical Property:

Vapor Pressure:0.00176mmHg at 25°C
Boiling Point:293.1°C at 760 mmHg
Flash Point:126°C
Density:1.017g/cm³
XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:200.120115130
Heavy Atom Count:15
Complexity:280

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(CC(=CC(=O)C1)C2=CC=CC=C2)C

Technology Process of 5,5-Dimethyl-3-phenyl-2-cyclohexen-1-one

There total 30 articles about 5,5-Dimethyl-3-phenyl-2-cyclohexen-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 92249-36-0
5,5-dimethyl-3-oxocyclohex-1-en-1-yl 4-nitrobenzenesulfonate

: 98-80-6
phenylboronic acid

: 36047-17-3
5,5-dimethyl-3-phenyl-2-cyclohexen-1-one

Guidance literature:: phenylboronic acid; With potassium carbonate; In tetrahydrofuran; water; for 0.0833333h; Inert atmosphere;

5,5-dimethyl-3-oxocyclohex-1-en-1-yl 4-nitrobenzenesulfonate; With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In tetrahydrofuran; water; at 30 ℃; for 1h; Inert atmosphere;
DOI:10.1002/chem.201300127

Reference yield: 98.0%

: 18369-65-8
3-acetyloxy-5,5-dimethyl-2-cyclohexenone

: 98-80-6
phenylboronic acid

: 36047-17-3
5,5-dimethyl-3-phenyl-2-cyclohexen-1-one

Guidance literature:: With tris(o-methoxyphenyl)phosphine; palladium diacetate; In water; acetone; at 22 ℃; for 18h; Reagent/catalyst; Solvent; Temperature; Catalytic behavior;
DOI:10.1002/anie.202006586

Reference yield: 90.0%

: 56671-85-3
5,5-dimethyl-3-iodocyclohex-2-en-1-one

: 98-80-6
phenylboronic acid

: 36047-17-3
5,5-dimethyl-3-phenyl-2-cyclohexen-1-one

Guidance literature:: With potassium fluoride; oxygen; diphenyl acetylene; palladium dichloride; In water; N,N-dimethyl-formamide; at 100 ℃; for 2h;
DOI:10.1021/ol0348349