5-Fluoro-2-nitro-N-phenylaniline

Base Information

Chemical Name:5-Fluoro-2-nitro-N-phenylaniline
CAS No.:322-68-9
Molecular Formula:C12H9FN2O2
Molecular Weight:232.214
Hs Code.:2921440000
Mol file:322-68-9.mol

Synonyms:

Suppliers and Price of 5-Fluoro-2-nitro-N-phenylaniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
5-Fluoro-2-nitro-N-phenylaniline
100mg
$ 65.00

Crysdot
5-Fluoro-2-nitro-N-phenylaniline 95+%
1g
$ 128.00

Crysdot
5-Fluoro-2-nitro-N-phenylaniline 95+%
5g
$ 494.00

American Custom Chemicals Corporation
5-FLUORO-2-NITRO-N-PHENYLANILINE 95.00%
1G
$ 271.95

AK Scientific
5-Fluoro-2-nitro-N-phenylaniline
5g
$ 744.00

Total 14 raw suppliers

Chemical Property of 5-Fluoro-2-nitro-N-phenylaniline

Chemical Property:

Melting Point:93-94 °C
Boiling Point:343.6±32.0 °C(Predicted)
PKA:-4.30±0.50(Predicted)
PSA：57.85000
Density:1.353±0.06 g/cm3(Predicted)
LogP:4.07370
Storage Temp.:2-8°C

Purity/Quality:

97% ^*data from raw suppliers

5-Fluoro-2-nitro-N-phenylaniline ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5-Fluoro-2-nitro-N-phenylaniline

There total 6 articles about 5-Fluoro-2-nitro-N-phenylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 446-35-5
2,4-Difluoronitrobenzene

: 62-53-3
aniline

: 322-68-9
4-fluoro-2-(phenylamino)nitrobenzene

Guidance literature:: aniline; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.5h; Inert atmosphere;

2,4-Difluoronitrobenzene; In tetrahydrofuran; at -78 ℃; for 1h;

With ammonium chloride; In tetrahydrofuran; water;

Reference yield: 71.0%

: 591-50-4
iodobenzene

: 2369-11-1
5-fluoro-2-nitroaniline

: 322-68-9
4-fluoro-2-(phenylamino)nitrobenzene

Guidance literature:: 5-fluoro-2-nitroaniline; With sodium t-butanolate; In toluene; for 1h; Inert atmosphere;

iodobenzene; With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tert-butyl phosphine; In toluene; at 60 ℃; Inert atmosphere;

Reference yield: 61.0%

: 62-53-3
aniline

: 350-46-9,178603-76-4
4-Fluoronitrobenzene

: 322-68-9
4-fluoro-2-(phenylamino)nitrobenzene

Guidance literature:: aniline; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.0166667h; Inert atmosphere;

4-Fluoronitrobenzene; In tetrahydrofuran; hexane; at -120 - -110 ℃; for 0.166667h; Inert atmosphere;

With potassium permanganate; ammonia; In tetrahydrofuran; hexane; at -110 ℃; for 0.0833333h; Inert atmosphere;
DOI:10.1039/c6cc02235a