1,4-Ditert-butyl-2,5-diiodobenzene

Base Information

Chemical Name:1,4-Ditert-butyl-2,5-diiodobenzene
CAS No.:3265-92-7
Molecular Formula:C14H20I2
Molecular Weight:
Hs Code.:
DSSTox Substance ID:DTXSID60409191
Wikidata:Q82214911
Mol file:3265-92-7.mol

Synonyms:1,4-ditert-butyl-2,5-diiodobenzene;3265-92-7;Benzene, 1,4-bis(1,1-dimethylethyl)-2,5-diiodo-;DTXSID60409191;AKOS024406202

Suppliers and Price of 1,4-Ditert-butyl-2,5-diiodobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 1,4-Ditert-butyl-2,5-diiodobenzene

Chemical Property:

XLogP3:6.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:2
Exact Mass:441.96545
Heavy Atom Count:16
Complexity:208

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(C)(C)C1=CC(=C(C=C1I)C(C)(C)C)I

Technology Process of 1,4-Ditert-butyl-2,5-diiodobenzene

There total 2 articles about 1,4-Ditert-butyl-2,5-diiodobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 22162-01-2
2,5-di-tert-butylbenzene-1,4-diamine

: 3265-92-7
1,4-di-tert-butyl-2,5-diiodobenzene

Guidance literature:: With sulfuric acid; acetic acid; potassium iodide; sodium nitrite;
DOI:10.1039/jr9580000120

Reference yield:

: 10472-70-5
2,5-di-tert-butyl-p-dinitrobenzene

: 3265-92-7
1,4-di-tert-butyl-2,5-diiodobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol; SnCl₂; aqueous HCl

2: sodium nitrite; sulfuric acid; acetic acid; aqueous potassium iodide solution

With hydrogenchloride; ethanol; sulfuric acid; acetic acid; potassium iodide; tin(ll) chloride; sodium nitrite;
DOI:10.1039/jr9580000120

Reference yield: 92.0%

: 3265-92-7
1,4-di-tert-butyl-2,5-diiodobenzene

: 1066-54-2
trimethylsilylacetylene

: 1609291-46-4
((2,5-di-tert-butyl-1,4-phenylene)bis(ethyne-2,1-diyl))bis(trimethylsilane)

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; at 50 ℃; for 10h; Inert atmosphere; Schlenk technique;
DOI:10.1039/c4cc02143f