1-(5-methoxy-2-methyl-1-benzofuran-3-yl)ethanone

Base Information

Chemical Name:1-(5-methoxy-2-methyl-1-benzofuran-3-yl)ethanone
CAS No.:33038-29-8
Molecular Formula:C12H12O3
Molecular Weight:204.22200
Hs Code.:

Synonyms:2-methyl-3-acetyl-5-methoxybenzofuran;1-(5-Methoxy-2-methyl-benzofuran-3-yl)-aethanon;1-(5-Methoxy-2-methyl-benzofuran-3-yl)-ethanone;3-acetyl-5-methoxy-2-methylbenzofuran;3-acetyl-5-methoxy-2-methylbenzo[b]furan;5-methoxy-3-acetyl-2-methylbenzofuran;

Suppliers and Price of 1-(5-methoxy-2-methyl-1-benzofuran-3-yl)ethanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-(5-methoxy-2-methyl-1-benzofuran-3-yl)ethanone

Chemical Property:

Melting Point:90 °C (butan-1-ol)
PSA：39.44000
LogP:2.95240

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-(5-methoxy-2-methyl-1-benzofuran-3-yl)ethanone

There total 8 articles about 1-(5-methoxy-2-methyl-1-benzofuran-3-yl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 28241-99-8
1-(5-hydroxy-2-methylbenzofuran-3-yl)ethan-1-one

: 74-88-4
methyl iodide

: 33038-29-8
1-(5-methoxy-2-methylbenzofuran-3-yl)ethanone

Guidance literature:: 1-(5-hydroxy-2-methylbenzofuran-3-yl)ethan-1-one; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 1h; Inert atmosphere;

methyl iodide; In N,N-dimethyl-formamide; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/ejoc.201001649

Reference yield: 74.0%

: 28241-99-8
1-(5-hydroxy-2-methylbenzofuran-3-yl)ethan-1-one

: 77-78-1
dimethyl sulfate

: 33038-29-8
1-(5-methoxy-2-methylbenzofuran-3-yl)ethanone

Guidance literature:: With sodium hydroxide; In 1,4-dioxane; for 2h;
DOI:10.1016/j.tetlet.2017.06.036

Reference yield:

: 123-54-6,81235-32-7
acetylacetone

: 33038-29-8
1-(5-methoxy-2-methylbenzofuran-3-yl)ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: zinc chloride; ethanol

2: aq. NaOH solution

With sodium hydroxide; ethanol; zinc(II) chloride;