1-Dichloromethoxy-4-methylbenzene

Base Information

• Chemical Name: 1-Dichloromethoxy-4-methylbenzene
• CAS No.: 33104-40-4
• Molecular Formula: C8H8Cl2O
• Molecular Weight: 191.057
• Mol file: 33104-40-4.mol

Synonyms:Dichloromethyl 4-tolyl ether;dichloromethyl 4-methylphenyl ether;Dichlormethyl-p-tolylaether;

Chemical Property of 1-Dichloromethoxy-4-methylbenzene

Chemical Property:

• PSA: 9.23000
• LogP: 3.13500

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Dichloromethoxy-4-methylbenzene

There total 3 articles about 1-Dichloromethoxy-4-methylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-cresol (106-44-5) + chloroform (67-66-3,8013-54-5) → p-tolyl formate (1864-97-7) + 2-hydroxy-5-methylbenzaldehyde (613-84-3) + dichloromethyl 4-methylphenyl ether (33104-40-4)

Guidance literature:

for 5h; Yield given. Yields of byproduct given; Irradiation;

DOI:10.1016/0040-4020(95)00235-Z

Reference yield:

p-tolyl formate (1864-97-7) → dichloromethyl 4-methylphenyl ether (33104-40-4)

Guidance literature:

With Dichloromethyl methyl ether; mercury dichloride; Heating;

Reference yield:

→ dichloromethyl 4-methylphenyl ether (33104-40-4)

Guidance literature:

upstream raw materials:

p-tolyl formate

p-cresol

chloroform

Downstream raw materials:

4-chloromethylphenyl dichloromethyl ether

4-methyl-α,α-difluoroanisole