2-CHLORO-N-(5-METHYL-BENZOTHIAZOL-2-YL)-ACETAMIDE

Base Information

• Chemical Name: 2-CHLORO-N-(5-METHYL-BENZOTHIAZOL-2-YL)-ACETAMIDE
• CAS No.: 3323-84-0
• Molecular Formula: C10H9ClN2OS
• Molecular Weight: 240.713
• Hs Code.: 2934200090
• Mol file: 3323-84-0.mol

Synonyms:3-chloroacetylamino-5-methyl isoxazole;2-Chloracetylamino-5-methylbenzothiazol;3-Chloracetylamino-5-methyl-isoxazol;

Chemical Property of 2-CHLORO-N-(5-METHYL-BENZOTHIAZOL-2-YL)-ACETAMIDE

Chemical Property:

• PSA: 73.72000
• LogP: 3.43150

Purity/Quality:

98%min ^*data from raw suppliers

2-Chloro-N-(5-methyl-benzothiazol-2-yl)-acetamide ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-CHLORO-N-(5-METHYL-BENZOTHIAZOL-2-YL)-ACETAMIDE

There total 2 articles about 2-CHLORO-N-(5-METHYL-BENZOTHIAZOL-2-YL)-ACETAMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

2-amino-5-methylbenzothiazole (14779-17-0) + chloroacetyl chloride (79-04-9) → N-(6-methylbenzothiazol-2-yl)-2-chloroacetamide (3323-84-0)

Guidance literature:

In acetic acid; at 10 - 30 ℃;

Reference yield:

(3-methylphenyl)thiourea (621-40-9) → N-(6-methylbenzothiazol-2-yl)-2-chloroacetamide (3323-84-0)

Guidance literature:

Multi-step reaction with 2 steps

1: bromine / CHCl₃

2: benzene / 2 h / Heating

With bromine; In chloroform; benzene;

Reference yield: 78.0%

N-(6-methylbenzothiazol-2-yl)-2-chloroacetamide (3323-84-0) + sodium 4-(3,4-dichlorophenyl)-1,2,3-thiadiazole-5-thiolate (1200398-09-9) → 2-{[4-(3,4-dichlorophenyl)-1,2,3-thiadiazol-5-yl]sulfanyl}-N-(5-methyl-1,3-benzothiazol-2-yl)acetamide (1200398-04-4)

Guidance literature:

In ethanol; at 20 ℃;

DOI:10.1002/cbdv.200900197

upstream raw materials:

2-amino-5-methylbenzothiazole

chloroacetyl chloride

(3-methylphenyl)thiourea

Downstream raw materials:

2-(4-(2,4-dibromophenyl)-1,2,3-thiadiazol-5-ylthio)-N-(5-methylbenzo[d]thiazol-2-yl)acetamide

2-(4-(3,4-dichlorophenyl)-1,2,3-selenadiazol-5-ylthio)-N-(5-methylbenzo[d]thiazol-2-yl)acetamide

4-amino-5-[2-(4-hydroxyphenyl)ethyl]-3-[N-(6-methylbenzothiazole-2-yl)acetamido]thio-4H-1,2,4-triazole

4-amino-5-(2-cyclohexylethyl)-3-[N-(6-methylbenzothiazole-2-yl)acetamido]thio-4H-1,2,4-triazole

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