Methyl 2-(2-forMyl-4-nitrophenoxy)hexanoate

Base Information

Chemical Name:Methyl 2-(2-forMyl-4-nitrophenoxy)hexanoate
CAS No.:335153-23-6
Molecular Formula:C14H17NO6
Molecular Weight:295.292
Hs Code.:
Mol file:335153-23-6.mol

Synonyms:methyl 2-(2-fluorophenyl)-2-methylpropionate;methyl 2-(2-formyl-4-nitro-phenoxy)-hexanoate;

Suppliers and Price of Methyl 2-(2-forMyl-4-nitrophenoxy)hexanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-(2-Formyl-4-nitrophenoxy)hexanoicAcidMethylEster
250mg
$ 165.00

ChemScene
methyl2-(2-formyl-4-nitrophenoxy)hexanoate
1g
$ 495.00

Total 14 raw suppliers

Chemical Property of Methyl 2-(2-forMyl-4-nitrophenoxy)hexanoate

Chemical Property:

Boiling Point:433.6±35.0 °C(Predicted)
PSA：98.42000
Density:1.231±0.06 g/cm3 (20 oC 760 Torr)
LogP:3.04110

Purity/Quality:

98%Min ^*data from raw suppliers

2-(2-Formyl-4-nitrophenoxy)hexanoicAcidMethylEster ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses Methyl 2-(2-forMyl-4-nitrophenoxy)hexanoate is used in the synthetic preparation of 7-Amino-4,5-dihydrobenzo[f][1,4]oxazepin-3-ones. 2-(2-Formyl-4-nitrophenoxy)hexanoic Acid Methyl Ester is used in the synthetic preparation of 7-Amino-4,5-dihydrobenzo[f][1,4]oxazepin-3-ones.

Technology Process of Methyl 2-(2-forMyl-4-nitrophenoxy)hexanoate

There total 4 articles about Methyl 2-(2-forMyl-4-nitrophenoxy)hexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.4%

: 138320-26-0
methyl 2-(2-formylphenoxy)hexanoate

: 335153-23-6
methyl 2-(2-formyl-4-nitrophenoxy)hexanoate

Guidance literature:: methyl 2-(2-formylphenoxy)hexanoate; With sulfuric acid; at 5 ℃; for 0.25h;

at 5 ℃; for 2h;

Reference yield: 87.0%

: 5445-19-2
methyl 2-bromohexanoate

: 97-51-8
5-Nitrosalicylaldehyde

: 335153-23-6
methyl 2-(2-formyl-4-nitrophenoxy)hexanoate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 92 - 94 ℃; for 3.5h;

Reference yield:

: 847869-79-8
methyl 2-(2-formyl-4-nitrophenoxy)butanoate

: 335153-23-6
methyl 2-(2-formyl-4-nitrophenoxy)hexanoate

Guidance literature:: Multi-step reaction with 2 steps

1: NaOH / 0.5 h / 90 °C

2: 87 percent / K₂CO₃ / dimethylformamide / 3.5 h / 92 - 94 °C

With sodium hydroxide; potassium carbonate; In N,N-dimethyl-formamide;