2,6,10,15-Tetraazahexadecanedioic acid, 6,10-bis[(phenylmethoxy)carbonyl]-, 16-(1,1-dimethylethyl) 1-(2,2,2-trichloroethyl) ester

Base Information

Chemical Name:2,6,10,15-Tetraazahexadecanedioic acid, 6,10-bis[(phenylmethoxy)carbonyl]-, 16-(1,1-dimethylethyl) 1-(2,2,2-trichloroethyl) ester
CAS No.:345898-28-4
Molecular Formula:C₃₄H₄₇Cl₃N₄O₈
Molecular Weight:746.128
Hs Code.:
Mol file:345898-28-4.mol

Synonyms:

Suppliers and Price of 2,6,10,15-Tetraazahexadecanedioic acid, 6,10-bis[(phenylmethoxy)carbonyl]-, 16-(1,1-dimethylethyl) 1-(2,2,2-trichloroethyl) ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,6,10,15-Tetraazahexadecanedioic acid, 6,10-bis[(phenylmethoxy)carbonyl]-, 16-(1,1-dimethylethyl) 1-(2,2,2-trichloroethyl) ester

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Technology Process of 2,6,10,15-Tetraazahexadecanedioic acid, 6,10-bis[(phenylmethoxy)carbonyl]-, 16-(1,1-dimethylethyl) 1-(2,2,2-trichloroethyl) ester

There total 10 articles about 2,6,10,15-Tetraazahexadecanedioic acid, 6,10-bis[(phenylmethoxy)carbonyl]-, 16-(1,1-dimethylethyl) 1-(2,2,2-trichloroethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: (3-{benzyloxycarbonyl-[3-(4-tert-butoxycarbonylamino-butylamino)-propyl]-amino}-propyl)-carbamic acid 2,2,2-trichloro-ethyl ester

: 345898-28-4
4,8-bis(benzyloxycarbonyl)-N¹-(2,2,2-trichloroethoxycarbonyl)-N¹²-(tert-butoxycarbonyl)-4,8-diaza-1,12-dodecanediamine

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 - 20 ℃; for 3.25h;
DOI:10.1246/bcsj.74.1743

Reference yield:

: 68076-36-8
1-amino-4-[(tert-butyloxycarbonyl)amino]butane

: 345898-28-4
4,8-bis(benzyloxycarbonyl)-N¹-(2,2,2-trichloroethoxycarbonyl)-N¹²-(tert-butoxycarbonyl)-4,8-diaza-1,12-dodecanediamine

Guidance literature:: Multi-step reaction with 3 steps

1: AcOH / methanol / 1 h / 20 °C

2: NaBH₃CN / methanol / 20 °C

3: 1.22 g / triethylamine / tetrahydrofuran / 3.25 h / 0 - 20 °C

With sodium cyanoborohydride; acetic acid; triethylamine; In tetrahydrofuran; methanol;
DOI:10.1246/bcsj.74.1743

Reference yield:

: 129392-85-4
N-t-butoxycarbonyl-4-azidobutylamine

: 345898-28-4
4,8-bis(benzyloxycarbonyl)-N¹-(2,2,2-trichloroethoxycarbonyl)-N¹²-(tert-butoxycarbonyl)-4,8-diaza-1,12-dodecanediamine

Guidance literature:: Multi-step reaction with 4 steps

1: 92.1 percent / PPh₃ / tetrahydrofuran; H₂O / 23 h / 0 - 20 °C

2: AcOH / methanol / 1 h / 20 °C

3: NaBH₃CN / methanol / 20 °C

4: 1.22 g / triethylamine / tetrahydrofuran / 3.25 h / 0 - 20 °C

With sodium cyanoborohydride; acetic acid; triethylamine; triphenylphosphine; In tetrahydrofuran; methanol; water;
DOI:10.1246/bcsj.74.1743