Tert-butyl N-(4-azidobutyl)carbamate

Base Information

• Chemical Name: Tert-butyl N-(4-azidobutyl)carbamate
• CAS No.: 129392-85-4
• Molecular Formula: C9H18N4O2
• Molecular Weight: 214.268
• DSSTox Substance ID: DTXSID30462652
• Nikkaji Number: J1.495.298E
• Mol file: 129392-85-4.mol

Synonyms:129392-85-4;Tert-butyl N-(4-azidobutyl)carbamate;4-Azido-N-Boc-1-butanamine;Carbamic acid, N-(4-azidobutyl)-, 1,1-dimethylethyl ester;Carbamic acid, (4-azidobutyl)-, 1,1-dimethylethyl ester;SCHEMBL15798200;DTXSID30462652;tert-Butyl(4-azidobutyl)carbamate;MFCD24452574;AKOS030239272;BP-29699;MS-21578;SY318740;FT-0710346;(4-Azido-butyl)-carbamic acid tert-butyl ester;F80687;EN300-7061928;A1-03090

Chemical Property of Tert-butyl N-(4-azidobutyl)carbamate

Chemical Property:

• PSA: 91.57000
• LogP: 2.25876
• XLogP3: 2.5
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 7
• Exact Mass: 214.14297583
• Heavy Atom Count: 15
• Complexity: 241

Purity/Quality:

98% ^*data from raw suppliers

(4-Azido-butyl)-carbamicacidtert-butylester 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(C)(C)OC(=O)NCCCCN=[N+]=[N-]

Technology Process of Tert-butyl N-(4-azidobutyl)carbamate

There total 9 articles about Tert-butyl N-(4-azidobutyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

di-tert-butyl dicarbonate (24424-99-5) + 4-azidobutan-1-amine (88192-20-5) → N-t-butoxycarbonyl-4-azidobutylamine (129392-85-4)

Guidance literature:

With sodium hydroxide; In tetrahydrofuran; water;

DOI:10.1016/S0040-4039(01)00282-9

Reference yield: 96.0%

N-(4-aminobutyl)carbaminsaeure-(tert-butyl)ester-hydrochlorid (33545-98-1) → N-t-butoxycarbonyl-4-azidobutylamine (129392-85-4)

Guidance literature:

With copper(ll) sulfate pentahydrate; triflic azide; potassium carbonate; In methanol; dichloromethane; water; at 20 ℃; for 20h;

DOI:10.1021/acs.bioconjchem.5b00644

Reference yield: 94.0%

tert-butyl 4-bromobutylcarbamate (164365-88-2) → N-t-butoxycarbonyl-4-azidobutylamine (129392-85-4)

Guidance literature:

With sodium azide; In N,N-dimethyl-formamide; at 60 ℃;

DOI:10.1039/c5ra12114k

upstream raw materials:

methanesulfonic acid 4-tert-butoxycarbonylaminobutyl ester

di-tert-butyl dicarbonate

4-azidobutan-1-amine

(4-hydroxybutyl)carbamic acid tert-butyl ester

Downstream raw materials:

1-amino-4-[(tert-butyloxycarbonyl)amino]butane

4,8-bis(benzyloxycarbonyl)-N¹-(2,2,2-trichloroethoxycarbonyl)-N¹²-(tert-butoxycarbonyl)-4,8-diaza-1,12-dodecanediamine

di-tert-butyl ((4,4'-(((4-sulfamoylphenethyl)azanediyl)bis(methylene))bis(1H-1,2,3-triazole-4,1-diyl))bis(butane-4,1-diyl))dicarbamate

4-azidobutan-1-amine hydrochloride

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 129392-85-4 tert-butyl (4-azidobutyl)carbamate

Send

Send

Metric Ton KG G Pound L ML

Send

Send