4-Methyl-2,3-dihydro-1H-cyclopenta[b]quinolin-4-ium iodide

Base Information

• Chemical Name: 4-Methyl-2,3-dihydro-1H-cyclopenta[b]quinolin-4-ium iodide
• CAS No.: 35005-74-4
• Molecular Formula: C13H14N.I
• DSSTox Substance ID: DTXSID10481664
• NSC Number: 239346

Synonyms:35005-74-4;NSC 239346;DTXSID10481664;4-Methyl-2,3-dihydro-1H-cyclopenta[b]quinolin-4-ium iodide;NSC239346;NSC-239346

Chemical Property of 4-Methyl-2,3-dihydro-1H-cyclopenta[b]quinolin-4-ium iodide

Chemical Property:

• Vapor Pressure: 0.000426mmHg at 25°C
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 311.01710
• Heavy Atom Count: 15
• Complexity: 213

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C[N+]1=C2CCCC2=CC3=CC=CC=C31.[I-]

Technology Process of 4-Methyl-2,3-dihydro-1H-cyclopenta[b]quinolin-4-ium iodide

There total 2 articles about 4-Methyl-2,3-dihydro-1H-cyclopenta[b]quinolin-4-ium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

2,3-dihydro-1H-cyclopenta[b]quinoline (5661-06-3) + methyl iodide (74-88-4) → N-methylcyclopentaquinolinium iodide (35005-74-4)

Guidance literature:

In acetone; for 18h; Ambient temperature;

DOI:10.1021/jo00004a029

Reference yield:

methyl iodide (74-88-4) → N-methylcyclopentaquinolinium iodide (35005-74-4)

Guidance literature:

Reference yield:

N-methylcyclopentaquinolinium iodide (35005-74-4) + p-dimethylaminonitrosobenzene (138-89-6) → 3-(4-dimethylamino-phenylimino)-4-methyl-2,3-dihydro-1H-cyclopenta[b]quinolinium; iodide

Guidance literature:

With piperidine; ethanol;

DOI:10.1039/jr9480001895

upstream raw materials:

2,3-dihydro-1H-cyclopenta[b]quinoline

methyl iodide

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