2,6-Bis(5,6-diphenyl-1,2,4-triazin-3-yl)pyridine

Base Information

Chemical Name:2,6-Bis(5,6-diphenyl-1,2,4-triazin-3-yl)pyridine
CAS No.:35171-28-9
Molecular Formula:C35H23N7
Molecular Weight:541.60400
Hs Code.:
European Community (EC) Number:660-653-8
Nikkaji Number:J2.953.263J
Mol file:35171-28-9.mol

Synonyms:2,6-bis(5,6-diphenyl-1,2,4-triazin-3-yl)pyridine;3-[6-(5,6-diphenyl-1,2,4-triazin-3-yl)pyridin-2-yl]-5,6-diphenyl-1,2,4-triazine;35171-28-9;SCHEMBL2486634;AKOS024434671;FT-0763544;2,6-Bis[5,6-diphenyl-1,2,4-triazine-3-yl]pyridine

Suppliers and Price of 2,6-Bis(5,6-diphenyl-1,2,4-triazin-3-yl)pyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
2,6-BIS(5,6-DIPHENYL-1,2,4-TRIAZIN-3-YL)PYRIDINE Aldrich
50mg
$ 144.00

American Custom Chemicals Corporation
2,6-BIS(5,6-DIPHENYL-1,2,4-TRIAZIN-3-YL)PYRIDINE 95.00%
5MG
$ 496.61

Total 2 raw suppliers

Chemical Property of 2,6-Bis(5,6-diphenyl-1,2,4-triazin-3-yl)pyridine

Chemical Property:

PSA：90.23000
LogP:7.45360
XLogP3:5.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:6
Exact Mass:541.20149376
Heavy Atom Count:42
Complexity:737

Purity/Quality:

99%, ^*data from raw suppliers

2,6-BIS(5,6-DIPHENYL-1,2,4-TRIAZIN-3-YL)PYRIDINE Aldrich ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C2=C(N=NC(=N2)C3=NC(=CC=C3)C4=NC(=C(N=N4)C5=CC=CC=C5)C6=CC=CC=C6)C7=CC=CC=C7

Technology Process of 2,6-Bis(5,6-diphenyl-1,2,4-triazin-3-yl)pyridine

There total 6 articles about 2,6-Bis(5,6-diphenyl-1,2,4-triazin-3-yl)pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 22538-57-4
pyridine-2,6-bis(carboximidehydrazide)

: 134-81-6
benzil

: 35171-28-9
2,6-bis-(5,6-diphenyl-1,2,4-triazin-3-yl)pyridine

Guidance literature:: In tetrahydrofuran; at 66 ℃; for 16h;
DOI:10.1002/jhet.2374

Reference yield: 88.0%

: 2,6-pyridine dicarboxamide dihydrazone

: 134-81-6
benzil

: 35171-28-9
2,6-bis-(5,6-diphenyl-1,2,4-triazin-3-yl)pyridine

Guidance literature:: With triethylamine; In 1,4-dioxane; for 72h; Reflux;
DOI:10.1039/d1dt00307k

Reference yield:

: 499-83-2
Pyridine-2,6-dicarboxylic acid

: 35171-28-9
2,6-bis-(5,6-diphenyl-1,2,4-triazin-3-yl)pyridine

Guidance literature:: Multi-step reaction with 5 steps

1: thionyl chloride / 14 h / 0 °C / Cooling with ice; Reflux

2: ammonia / water / 1 h / 40 °C

3: trichlorophosphate / N,N-dimethyl-formamide / 0 - 20 °C

4: hydrazine hydrate / ethanol / 336 - 360 h / 20 °C

5: triethylamine / 1,4-dioxane / 72 h / Reflux

With thionyl chloride; ammonia; hydrazine hydrate; triethylamine; trichlorophosphate; In 1,4-dioxane; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1039/d1dt00307k