N-Methoxy-N-methyl-1-phenylmethanamine

Base Information

Chemical Name:N-Methoxy-N-methyl-1-phenylmethanamine
CAS No.:3555-65-5
Molecular Formula:C9H13NO
Molecular Weight:151.208
Hs Code.:
DSSTox Substance ID:DTXSID30571470
Wikidata:Q82459560
Mol file:3555-65-5.mol

Synonyms:N-Methoxy-N-methyl-1-phenylmethanamine;3555-65-5;SCHEMBL112375;benzyl-N,O-dimethylhydroxylamine;DTXSID30571470

Suppliers and Price of N-Methoxy-N-methyl-1-phenylmethanamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of N-Methoxy-N-methyl-1-phenylmethanamine

Chemical Property:

XLogP3:2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:151.099714038
Heavy Atom Count:11
Complexity:99.7

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(CC1=CC=CC=C1)OC

Technology Process of N-Methoxy-N-methyl-1-phenylmethanamine

There total 5 articles about N-Methoxy-N-methyl-1-phenylmethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 6919-61-5
N-methoxy-N-methylbenzamide

: 3555-65-5
N-benzyl-N,O-dimethylhydroxylamine

Guidance literature:: With 9-borabicyclo[3.3.1]nonane; In tetrahydrofuran; at 25 ℃; for 1h; Inert atmosphere;
DOI:10.1021/acs.joc.6b00276

Reference yield:

: 6919-61-5
N-methoxy-N-methylbenzamide

: 3555-65-5
N-benzyl-N,O-dimethylhydroxylamine

: 100-51-6,185532-71-2
benzyl alcohol

Guidance literature:: With 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane; In neat (no solvent); at 120 ℃; for 24h; Inert atmosphere; Sealed tube;
DOI:10.1002/bkcs.12438

Reference yield:

: 98-88-4
benzoyl chloride

: 3555-65-5
N-benzyl-N,O-dimethylhydroxylamine

: 100-51-6,185532-71-2
benzyl alcohol

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 0 - 25 °C

2: 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane / neat (no solvent) / 24 h / 120 °C / Inert atmosphere; Sealed tube

With triethylamine; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane; In dichloromethane;
DOI:10.1002/bkcs.12438