1-(benzo[d][1,3]dioxol-5-yl)-2-(6-Methylpyridin-2-yl)ethanone

Base Information

Chemical Name:1-(benzo[d][1,3]dioxol-5-yl)-2-(6-Methylpyridin-2-yl)ethanone
CAS No.:356560-89-9
Molecular Formula:C₁₅H₁₃NO₃
Molecular Weight:255.273
Hs Code.:
Mol file:356560-89-9.mol

Synonyms:1-Benzo[1,3]dioxol-5-yl-2-(6-methyl-pyridin-2-yl)-ethanone;1-benzo[1,3]dioxol-5-yl-2-(6-methylpyridin-2-yl)ethanone;1-(benzo[1,3]dioxol-5-yl)-2-(6-methylpyridin-2-yl)-ethanone;

Suppliers and Price of 1-(benzo[d][1,3]dioxol-5-yl)-2-(6-Methylpyridin-2-yl)ethanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 4 raw suppliers

Chemical Property of 1-(benzo[d][1,3]dioxol-5-yl)-2-(6-Methylpyridin-2-yl)ethanone

Chemical Property:

PSA：48.42000
LogP:2.54410

Purity/Quality:: 99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-(benzo[d][1,3]dioxol-5-yl)-2-(6-Methylpyridin-2-yl)ethanone

There total 3 articles about 1-(benzo[d][1,3]dioxol-5-yl)-2-(6-Methylpyridin-2-yl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 108-48-5
2,6-dimethylpyridine

: 147030-72-6
benzo[1,3]dioxole-5-carboxylic acid methoxymethylamide

: 356560-89-9
1-(benzo[1,3]dioxol-5-yl)-2-(6-methylpyridin-2-yl)ethanone

Guidance literature:: 2,6-dimethylpyridine; benzo[1,3]dioxole-5-carboxylic acid methoxymethylamide; With lithium diisopropyl amide; In tetrahydrofuran; hexanes; at -78 - 20 ℃; for 2h;

With ammonium chloride; In tetrahydrofuran; hexanes; water;

Reference yield: 79.0%

: 108-48-5
2,6-dimethylpyridine

: 6951-08-2
ethyl 1,3-benzodioxole-5-carboxylate

: 356560-89-9
1-(benzo[1,3]dioxol-5-yl)-2-(6-methylpyridin-2-yl)ethanone

Guidance literature:: With sodium hexamethyldisilazane; In tetrahydrofuran; at -20 - 20 ℃;

Reference yield: 76.0%

: 108-48-5
2,6-dimethylpyridine

: 326-56-7
methyl 3,4-methylenedioxybenzoate

: 356560-89-9
1-(benzo[1,3]dioxol-5-yl)-2-(6-methylpyridin-2-yl)ethanone

Guidance literature:: 2,6-dimethylpyridine; With lithium hexamethyldisilazane; In tetrahydrofuran; at -60 ℃;

methyl 3,4-methylenedioxybenzoate; In tetrahydrofuran; at -60 ℃; for 0.333333h; Further stages.;
DOI:10.1021/jm070129k DOI:10.1016/j.bmcl.2008.01.084