Hydrazinecarboxylic acid, (1S,2R,5S)-5-methyl-2-(1-methylethyl)cyclohexyl ester

Base Information

Chemical Name:Hydrazinecarboxylic acid, (1S,2R,5S)-5-methyl-2-(1-methylethyl)cyclohexyl ester
CAS No.:357219-75-1
Molecular Formula:C11H22N2O2
Molecular Weight:214.30500
Hs Code.:
Mol file:357219-75-1.mol

Synonyms:(?)-menthyl-carbazate;(-)-menthyl carbazaete;L-(+)-menthydrazide;Hydrazinecarboxylic acid (1S,2R,5S)-2-isopropyl-5-methyl-cyclohexyl ester;

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Hydrazinecarboxylic acid, (1S,2R,5S)-5-methyl-2-(1-methylethyl)cyclohexyl ester

Chemical Property:

Boiling Point:333.2±9.0 °C(Predicted)
PSA：64.35000
Density:1.02±0.1 g/cm3(Predicted)
LogP:3.13830

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Hydrazinecarboxylic acid, (1S,2R,5S)-5-methyl-2-(1-methylethyl)cyclohexyl ester

There total 2 articles about Hydrazinecarboxylic acid, (1S,2R,5S)-5-methyl-2-(1-methylethyl)cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 67714-24-3
(-)-menthyl phenyl carbonate

: 357219-75-1
(-)-menthyl N-aminocarbamate

Guidance literature:: With hydrazine hydrate; In ethanol; for 1h; Heating;
DOI:10.1016/S0040-4020(01)85944-5

Reference yield:

: 2216-51-5
(-)-menthol

: 357219-75-1
(-)-menthyl N-aminocarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / pyridine / in ice bath, then room t.

2: 95 percent / hydrazine hydrate / ethanol / 1 h / Heating

With pyridine; hydrazine hydrate; In ethanol;
DOI:10.1016/S0040-4020(01)85944-5

Reference yield: 45.0%

: (η(5)-C5H4COMe)(CO)2MoFeCo(μ3-S)(CO)6

: 357219-75-1
(-)-menthyl N-aminocarbamate

: (μ3-S)CoMoFe(CO)8[η5-C5H4C(NNHCO2-menthyl)Me]

Guidance literature:: With sulfuric acid; In ethanol; (N2); drops of H2SO4 used; stirred at room temp. for 12 h; condensed, the residue chromd. (SiO2, hexane/CH2Cl2, then hexane/CH2Cl2/ether), solvent-removed, crystd. at -20°C from CH2Cl2/hexane; elem. anal.;
DOI:10.1016/S0020-1693(01)00650-8