4-Methoxy-2-naphthylamine

Base Information

• Chemical Name: 4-Methoxy-2-naphthylamine
• CAS No.: 2764-95-6
• Molecular Formula: C11H11NO
• Molecular Weight: 173.214
• Hs Code.: 2922199090
• European Community (EC) Number: 686-490-2
• DSSTox Substance ID: DTXSID60182018
• Nikkaji Number: J264.852K
• Wikidata: Q27462320
• Mol file: 2764-95-6.mol

Synonyms:4-methoxy beta-naphthylamine;4-methoxy-2-naphthylamine

Chemical Property of 4-Methoxy-2-naphthylamine

Chemical Property:

• Vapor Pressure: 3.72E-05mmHg at 25°C
• Melting Point: 57.5-58.5 °C(Solv: ligroine (8032-32-4))
• Refractive Index: 1.655
• Boiling Point: 352.9 °C at 760 mmHg
• PKA: 4.06±0.10(Predicted)
• Flash Point: 186.9 °C
• PSA: 35.25000
• Density: 1.156g/cm³
• LogP: 3.01180
• Storage Temp.: −20°C
• XLogP3: 2.9
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 1
• Exact Mass: 173.084063974
• Heavy Atom Count: 13
• Complexity: 172

Purity/Quality:

97% ^*data from raw suppliers

4-Methoxy-2-naphthylamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Chemical Classes: Nitrogen Compounds -> Naphthylamines
• Canonical SMILES: COC1=CC(=CC2=CC=CC=C21)N

Technology Process of 4-Methoxy-2-naphthylamine

There total 19 articles about 4-Methoxy-2-naphthylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

glycyl-prolyl-4-methoxy-β-naphthylamide (42761-76-2) → 4-methoxy-2-naphthylamine (2764-95-6) + H-Gly-Pro-OH (704-15-4)

Guidance literature:

With dipeptidyl peptidase IV; at 40 ℃; Product distribution;

Reference yield:

ethyl 4-methoxy-2-naphthalenecarbamate (90072-95-0) → 4-methoxy-2-naphthylamine (2764-95-6)

Guidance literature:

With potassium hydroxide; In ethylene glycol; at 160 ℃; for 1.5h;

Reference yield:

1-Methoxy-3-nitronaphthalene (13802-40-9) → 4-methoxy-2-naphthylamine (2764-95-6)

Guidance literature:

With methanol; palladium on activated charcoal; Hydrogenation;

DOI:10.1021/ja01543a029

upstream raw materials:

1-Methoxy-3-nitronaphthalene

ethyl 4-methoxy-2-naphthalenecarbamate

3-Acetamido-1-methoxy-naphthalin

chloro-2 methoxy-1 naphtalene

Downstream raw materials:

N-benzyloxycarbonyl-L-leucine-(4-methoxy-[2]naphthylamide)

L-alanine-4-methoxy-2-naphthylamide hydrochloride

<3-(2-Amino-4-methoxy-naphthalin-1-azo)-phenyl>-<2,5-diaethoxy-4-benzamino-benzoldiazo>-thioaether

<4-(2-Amino-4-methoxy-naphthalin-1-azo)-phenyl>-2,5-diaethoxy-4-benzamino)-benzoldiazo>-thioaether

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