Carbonic acid, 1,1-dimethylethyl 2-hexyl-6-iodo-4-[[tris(1-methylethyl)silyl]ethynyl]phenyl ester

Base Information

Chemical Name:Carbonic acid, 1,1-dimethylethyl 2-hexyl-6-iodo-4-[[tris(1-methylethyl)silyl]ethynyl]phenyl ester
CAS No.:364068-92-8
Molecular Formula:C28H45IO3Si
Molecular Weight:584.654
Hs Code.:

Synonyms:

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Chemical Property of Carbonic acid, 1,1-dimethylethyl 2-hexyl-6-iodo-4-[[tris(1-methylethyl)silyl]ethynyl]phenyl ester

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Technology Process of Carbonic acid, 1,1-dimethylethyl 2-hexyl-6-iodo-4-[[tris(1-methylethyl)silyl]ethynyl]phenyl ester

There total 5 articles about Carbonic acid, 1,1-dimethylethyl 2-hexyl-6-iodo-4-[[tris(1-methylethyl)silyl]ethynyl]phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3226-32-2
2-hexylphenol

: 364068-92-8
carbonic acid tert-butyl ester 2-hexyl-6-iodo-4-[(triisopropylsilanyl)-ethynyl]-phenyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 17.3 g / iodine monochloride; Et₃N / CH₂Cl₂ / 3.5 h / 0 °C

2: 85 percent / Et₃N; DMAP / CH₂Cl₂ / 1 h / 0 °C

3: 69 percent / CuI; PPh₃; Et₃N / Pd(OAc)2 / 72 h / 20 °C

4: NaOH / methanol; tetrahydrofuran / 20 °C

5: 5.4 g / K₂CO₃; DMAP; [18]crown-6 / tetrahydrofuran / 1 h

With dmap; sodium hydroxide; copper(l) iodide; 18-crown-6 ether; Iodine monochloride; potassium carbonate; triethylamine; triphenylphosphine; palladium diacetate; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1002/chem.200305284

Reference yield:

: 81693-79-0
2-n-hexyl-1-methoxybenzene

: 364068-92-8
carbonic acid tert-butyl ester 2-hexyl-6-iodo-4-[(triisopropylsilanyl)-ethynyl]-phenyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: boron tribromide / CH₂Cl₂

2: 17.3 g / iodine monochloride; Et₃N / CH₂Cl₂ / 3.5 h / 0 °C

3: 85 percent / Et₃N; DMAP / CH₂Cl₂ / 1 h / 0 °C

4: 69 percent / CuI; PPh₃; Et₃N / Pd(OAc)2 / 72 h / 20 °C

5: NaOH / methanol; tetrahydrofuran / 20 °C

6: 5.4 g / K₂CO₃; DMAP; [18]crown-6 / tetrahydrofuran / 1 h

With dmap; sodium hydroxide; copper(l) iodide; 18-crown-6 ether; Iodine monochloride; boron tribromide; potassium carbonate; triethylamine; triphenylphosphine; palladium diacetate; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1002/chem.200305284

Reference yield:

: 364068-89-3
2-hexyl-4,6-diiodo-phenol

: 364068-92-8
carbonic acid tert-butyl ester 2-hexyl-6-iodo-4-[(triisopropylsilanyl)-ethynyl]-phenyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / Et₃N; DMAP / CH₂Cl₂ / 1 h / 0 °C

2: 69 percent / CuI; PPh₃; Et₃N / Pd(OAc)2 / 72 h / 20 °C

3: NaOH / methanol; tetrahydrofuran / 20 °C

4: 5.4 g / K₂CO₃; DMAP; [18]crown-6 / tetrahydrofuran / 1 h

With dmap; sodium hydroxide; copper(l) iodide; 18-crown-6 ether; potassium carbonate; triethylamine; triphenylphosphine; palladium diacetate; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1002/chem.200305284