Carbonic acid, 4-[[2-[[(1,1-dimethylethoxy)carbonyl]oxy]-5-ethynyl-3-hexylphenyl]ethynyl] -2-hexyl-6-(phenylethynyl)phenyl 1,1-dimethylethyl ester

Base Information

Chemical Name:Carbonic acid, 4-[[2-[[(1,1-dimethylethoxy)carbonyl]oxy]-5-ethynyl-3-hexylphenyl]ethynyl] -2-hexyl-6-(phenylethynyl)phenyl 1,1-dimethylethyl ester
CAS No.:364068-94-0
Molecular Formula:C46H54O6
Molecular Weight:702.931
Hs Code.:

Carbonic acid,
4-[[2-[[(1,1-dimethylethoxy)carbonyl]oxy]-5-ethynyl-3-hexylphenyl]ethynyl]
-2-hexyl-6-(phenylethynyl)phenyl 1,1-dimethylethyl ester

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Chemical Property of Carbonic acid, 4-[[2-[[(1,1-dimethylethoxy)carbonyl]oxy]-5-ethynyl-3-hexylphenyl]ethynyl] -2-hexyl-6-(phenylethynyl)phenyl 1,1-dimethylethyl ester

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Technology Process of Carbonic acid, 4-[[2-[[(1,1-dimethylethoxy)carbonyl]oxy]-5-ethynyl-3-hexylphenyl]ethynyl] -2-hexyl-6-(phenylethynyl)phenyl 1,1-dimethylethyl ester

There total 10 articles about Carbonic acid, 4-[[2-[[(1,1-dimethylethoxy)carbonyl]oxy]-5-ethynyl-3-hexylphenyl]ethynyl] -2-hexyl-6-(phenylethynyl)phenyl 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3226-32-2
2-hexylphenol

: 364068-94-0
C₄₆H₅₄O₆

Guidance literature:: Multi-step reaction with 7 steps

1: 17.3 g / iodine monochloride; Et₃N / CH₂Cl₂ / 3.5 h / 0 °C

2: 85 percent / Et₃N; DMAP / CH₂Cl₂ / 1 h / 0 °C

3: 69 percent / CuI; PPh₃; Et₃N / Pd(OAc)2 / 72 h / 20 °C

4: NaOH / methanol; tetrahydrofuran / 20 °C

5: 5.4 g / K₂CO₃; DMAP; [18]crown-6 / tetrahydrofuran / 1 h

6: CuI; PPh₃; Et₃N / Pd(OAc)2 / 6 h / 70 °C

7: 1.96 g / tetrabutylammonium fluoride / CH₂Cl₂; tetrahydrofuran

With dmap; sodium hydroxide; copper(l) iodide; 18-crown-6 ether; tetrabutyl ammonium fluoride; Iodine monochloride; potassium carbonate; triethylamine; triphenylphosphine; palladium diacetate; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1002/chem.200305284

Reference yield:

: 81693-79-0
2-n-hexyl-1-methoxybenzene

: 364068-94-0
C₄₆H₅₄O₆

Guidance literature:: Multi-step reaction with 8 steps

1: boron tribromide / CH₂Cl₂

2: 17.3 g / iodine monochloride; Et₃N / CH₂Cl₂ / 3.5 h / 0 °C

3: 85 percent / Et₃N; DMAP / CH₂Cl₂ / 1 h / 0 °C

4: 69 percent / CuI; PPh₃; Et₃N / Pd(OAc)2 / 72 h / 20 °C

5: NaOH / methanol; tetrahydrofuran / 20 °C

6: 5.4 g / K₂CO₃; DMAP; [18]crown-6 / tetrahydrofuran / 1 h

7: CuI; PPh₃; Et₃N / Pd(OAc)2 / 6 h / 70 °C

8: 1.96 g / tetrabutylammonium fluoride / CH₂Cl₂; tetrahydrofuran

With dmap; sodium hydroxide; copper(l) iodide; 18-crown-6 ether; tetrabutyl ammonium fluoride; Iodine monochloride; boron tribromide; potassium carbonate; triethylamine; triphenylphosphine; palladium diacetate; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1002/chem.200305284

Reference yield:

: 364068-89-3
2-hexyl-4,6-diiodo-phenol

: 364068-94-0
C₄₆H₅₄O₆

Guidance literature:: Multi-step reaction with 6 steps

1: 85 percent / Et₃N; DMAP / CH₂Cl₂ / 1 h / 0 °C

2: 69 percent / CuI; PPh₃; Et₃N / Pd(OAc)2 / 72 h / 20 °C

3: NaOH / methanol; tetrahydrofuran / 20 °C

4: 5.4 g / K₂CO₃; DMAP; [18]crown-6 / tetrahydrofuran / 1 h

5: CuI; PPh₃; Et₃N / Pd(OAc)2 / 6 h / 70 °C

6: 1.96 g / tetrabutylammonium fluoride / CH₂Cl₂; tetrahydrofuran

With dmap; sodium hydroxide; copper(l) iodide; 18-crown-6 ether; tetrabutyl ammonium fluoride; potassium carbonate; triethylamine; triphenylphosphine; palladium diacetate; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1002/chem.200305284