CARBAMIC ACID, N-(2-BROMO-4-METHYLPHENYL)-, 1,1-DIMETHYLETHYL ESTER

Base Information

Chemical Name:CARBAMIC ACID, N-(2-BROMO-4-METHYLPHENYL)-, 1,1-DIMETHYLETHYL ESTER
CAS No.:364607-53-4
Molecular Formula:C12H16BrNO2
Molecular Weight:286.169
Hs Code.:2921430090
Mol file:364607-53-4.mol

Synonyms:N-BOC-2-bromo-4-methylaniline;2-Bromo-4-fluorobenzyl Alcohol;tert-butyl 2-bromo-4-methylphenylcarbamate;

Suppliers and Price of CARBAMIC ACID, N-(2-BROMO-4-METHYLPHENYL)-, 1,1-DIMETHYLETHYL ESTER

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
N-BOC2-Bromo-4-methylaniline
500mg
$ 325.00

TRC
N-BOC2-Bromo-4-methylaniline
250mg
$ 210.00

Labseeker
Carbamicacid,N-(2-bromo-4-methylphenyl)-,1,1-dimethylethylester 95
100g
$ 3300.00

Crysdot
N-BOC2-Bromo-4-methylaniline 95+%
5g
$ 790.00

AK Scientific
N-BOC2-Bromo-4-methylaniline
5g
$ 1171.00

Total 1 raw suppliers

Chemical Property of CARBAMIC ACID, N-(2-BROMO-4-METHYLPHENYL)-, 1,1-DIMETHYLETHYL ESTER

Chemical Property:

PSA：41.82000
LogP:4.11810

Purity/Quality:: N-BOC2-Bromo-4-methylaniline ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of CARBAMIC ACID, N-(2-BROMO-4-METHYLPHENYL)-, 1,1-DIMETHYLETHYL ESTER

There total 4 articles about CARBAMIC ACID, N-(2-BROMO-4-METHYLPHENYL)-, 1,1-DIMETHYLETHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 24424-99-5
di-tert-butyl dicarbonate

2-bromo-p-toluidine: 583-68-6
2-bromo-p-toluidine

: 364607-53-4
(2-bromo-4-methyl-phenyl)-carbamic acid tert-butyl ester

Guidance literature:: In tetrahydrofuran; for 24h; Heating;
DOI:10.1021/jo800914c

Reference yield: 87.0%

: 14618-59-8
N-(tert-butoxycarbonyl)-4-methylaniline

: 364607-53-4
(2-bromo-4-methyl-phenyl)-carbamic acid tert-butyl ester

Guidance literature:: With N-Bromosuccinimide; palladium diacetate; toluene-4-sulfonic acid; In 1,2-dichloro-ethane; at 60 ℃; for 16h; regioselective reaction; Sealed tube;
DOI:10.1021/acs.joc.6b00329

Reference yield: 78.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 29289-13-2
2-iodo-4-methylaniline

: 364607-53-4
(2-bromo-4-methyl-phenyl)-carbamic acid tert-butyl ester

Guidance literature:: 2-iodo-4-methylaniline; With sodium hexamethyldisilazane; In tetrahydrofuran; at 20 ℃; for 0.416667h;

di-tert-butyl dicarbonate; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1002/adsc.201300338