3-Hexanone, 5-hydroxy-2,5-dimethyl-

Base Information

Chemical Name:3-Hexanone, 5-hydroxy-2,5-dimethyl-
CAS No.:36587-79-8
Molecular Formula:C8H16O2
Molecular Weight:144.21100
Hs Code.:
Mol file:36587-79-8.mol

Synonyms:5-Hydroxy-2,5-dimethyl-hexan-3-on;5-hydroxy-2,5-dimethyl-hexan-3-one;2.5-Dimethyl-hexanol-(5)-on-(3);5-hydroxy-2,5-dimethyl-3-hexanone;3-Hexanone,5-hydroxy-2,5-dimethyl;

Suppliers and Price of 3-Hexanone, 5-hydroxy-2,5-dimethyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 3-Hexanone, 5-hydroxy-2,5-dimethyl-

Chemical Property:

PSA：37.30000
LogP:1.37250

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-Hexanone, 5-hydroxy-2,5-dimethyl-

There total 1 articles about 3-Hexanone, 5-hydroxy-2,5-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 563-80-4
3-methyl-butan-2-one

: 67-64-1
acetone

: 36587-79-8
5-hydroxy-2,5-dimethyl-3-hexanone

Guidance literature:: 3-methyl-butan-2-one; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 1h;

acetone; In tetrahydrofuran; at -78 ℃; for 3h;
DOI:10.1002/chem.200400951

Reference yield:

: 36587-79-8
5-hydroxy-2,5-dimethyl-3-hexanone

: 36471-61-1,103668-43-5,54877-01-9,65534-62-5,125873-95-2,128899-83-2
racem. 2,6-dimethyl-heptane-3,5-diol

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / Zr(O-t-Bu)4 / CH₂Cl₂ / 3 h / 0 °C

2: 100 percent / KOH / methanol / 24 h / 20 °C

With potassium hydroxide; zirconium(IV) tert-butoxide; In methanol; dichloromethane; 1: aldol-Tishchenko reaction;
DOI:10.1002/chem.200400951