Tetracyclo[6.6.2.02,7.09,14]hexadecane-2(7),3,5,9(14),10,12-hexene-15,15,16,16-tetracarbonitrile

Base Information

• Chemical Name: Tetracyclo[6.6.2.02,7.09,14]hexadecane-2(7),3,5,9(14),10,12-hexene-15,15,16,16-tetracarbonitrile
• CAS No.: 1625-84-9
• Molecular Formula: C20H10 N4
• Molecular Weight: 306.326
• Hs Code.: 2926909090
• Mol file: 1625-84-9.mol

Synonyms:1,1,12,12-Tetracyano-9,10-dihydro-9,10-ethanoanthracene;NSC 42839

Chemical Property of Tetracyclo[6.6.2.02,7.09,14]hexadecane-2(7),3,5,9(14),10,12-hexene-15,15,16,16-tetracarbonitrile

Chemical Property:

• Vapor Pressure: 5.49E-17mmHg at 25°C
• Boiling Point: 654.1°Cat760mmHg
• Flash Point: 329.4°C
• PSA: 95.16000
• Density: 1.39g/cm³
• LogP: 3.34452

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Tetracyclo[6.6.2.02,7.09,14]hexadecane-2(7),3,5,9(14),10,12-hexene-15,15,16,16-tetracarbonitrile

There total 11 articles about Tetracyclo[6.6.2.02,7.09,14]hexadecane-2(7),3,5,9(14),10,12-hexene-15,15,16,16-tetracarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

9,10-dihydroanthracene (613-31-0) + ethenetetracarbonitrile (670-54-2) → 9,10-dihydro-9,10-ethano-anthracene-11,11,12,12-tetracarbonitrile (1625-84-9)

Guidance literature:

In dichloromethane;

DOI:10.1016/0022-328X(90)85360-B

Reference yield: 9.0%

anthracene (120-12-7) + 5,5,6,6-tetracyano-2-thiabicyclo<2.2.0>hexane (94732-90-8) → 9,10-dihydro-9,10-ethano-anthracene-11,11,12,12-tetracarbonitrile (1625-84-9) + 3-amino-4-cyano-2-(2,2-dicyanovinyl)thiophene (94732-91-9)

Guidance literature:

In acetonitrile; for 12h; Heating;

DOI:10.1021/jo00206a014

Reference yield:

anthracene (120-12-7) + ethenetetracarbonitrile (670-54-2) → 9,10-dihydro-9,10-ethano-anthracene-11,11,12,12-tetracarbonitrile (1625-84-9)

Guidance literature:

In 1,4-dioxane; at 25 ℃; Rate constant; Equilibrium constant; Thermodynamic data; var. solvents; kinetics, ΔH(excit.), ΔS(excit.);

upstream raw materials:

anthracene

ethenetetracarbonitrile

9,10-dihydroanthracene

5,6,11,12-tetrahydro-5,12;6,11-di-o-benzeno-dibenzo[a,e]cyclooctene

Downstream raw materials:

anthracene

ethenetetracarbonitrile