Benzenamine, 4-bromo-N,N-bis(trifluoromethyl)-

Base Information

• Chemical Name: Benzenamine, 4-bromo-N,N-bis(trifluoromethyl)-
• CAS No.: 3700-35-4
• Molecular Formula: C8H4BrF6N
• Molecular Weight: 308.021
• Hs Code.: 2921420090
• Mol file: 3700-35-4.mol

Synonyms:N.N-Bis-trifluormethyl-4-brom-anilin;4-bromo-NN-bistrifluoromethylaniline;

Chemical Property of Benzenamine, 4-bromo-N,N-bis(trifluoromethyl)-

Chemical Property:

• PSA: 3.24000
• LogP: 4.29510

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenamine, 4-bromo-N,N-bis(trifluoromethyl)-

There total 1 articles about Benzenamine, 4-bromo-N,N-bis(trifluoromethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 4.0%

bromobenzene (108-86-1,52753-63-6) + perfluoro(2,4-dimethyl-3-oxa-2,4-diazapentane) (6141-72-6) → p-bromo-N,N-bis(trifluoromethyl)aniline (3700-35-4) + O-[4-(Bis-trifluoromethyl-amino)-phenyl]-N,N-bis-trifluoromethyl-hydroxylamine + m-bromo-N,N-bis(trifluoromethyl)aniline + (2-Bromo-phenyl)-bis-trifluoromethyl-amine

Guidance literature:

for 432h; Ambient temperature;

DOI:10.1016/S0022-1139(00)85077-0

Reference yield: 83.0%

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + p-bromo-N,N-bis(trifluoromethyl)aniline (3700-35-4) → C17H12F6

Guidance literature:

With palladium diacetate; potassium carbonate; acetylacetone; In N,N-dimethyl-formamide; at 130 ℃; for 1h; Inert atmosphere;

DOI:10.1016/j.jfluchem.2011.10.014

Reference yield:

p-bromo-N,N-bis(trifluoromethyl)aniline (3700-35-4) → N,N-bis(trifluoromethyl)aniline (3700-19-4)

Guidance literature:

With copper; zinc; In water; acetone; at 20 ℃; for 24h;

DOI:10.1016/j.jfluchem.2011.10.014

upstream raw materials:

bromobenzene

perfluoro(2,4-dimethyl-3-oxa-2,4-diazapentane)

Downstream raw materials:

p-N,N-bis(trifluoromethyl)aminobenzaldehyde

1-<(4-NN-bistrifluoromethylamino)phenyl>-2-nitroprop-1-ene

N,N-bis(trifluoromethyl)aniline